L-Phenylalanine, 4-[(2-chloroethyl)amino]-

Base Information

Chemical Name:L-Phenylalanine, 4-[(2-chloroethyl)amino]-
CAS No.:573704-41-3
Molecular Formula:C11H15ClN2O2
Molecular Weight:242.705
Hs Code.:

Synonyms:

Suppliers and Price of L-Phenylalanine, 4-[(2-chloroethyl)amino]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of L-Phenylalanine, 4-[(2-chloroethyl)amino]-

Chemical Property:

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Technology Process of L-Phenylalanine, 4-[(2-chloroethyl)amino]-

There total 6 articles about L-Phenylalanine, 4-[(2-chloroethyl)amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1374033-39-2
4-[(2'-chloroethyl)amino]-N-boc-L-phenylalanine

: 573704-41-3
C₁₁H₁₅ClN₂O₂

Guidance literature:: 4-[(2'-chloroethyl)amino]-N-boc-L-phenylalanine; With hydrogenchloride; water; In ethyl acetate; for 3h;

With potassium carbonate; In isopropyl alcohol; for 3h; Product distribution / selectivity; Cooling with ice;

Reference yield:

: 17193-40-7
(S)-4-nitrophenylalanine methyl ester hydrochloride

: 573704-41-3
C₁₁H₁₅ClN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 4 h / 3102.97 Torr

3.1: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide; ethanol; water / 2 h

4.1: water; lithium hydroxide / methanol / 0 °C

4.2: pH 4

5.1: hydrogenchloride; water / ethyl acetate / 3 h

5.2: 3 h / Cooling with ice

With hydrogenchloride; water; hydrogen; sodium cyanoborohydride; acetic acid; triethylamine; lithium hydroxide; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 65615-89-6
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(4-nitrophenyl)propanoate

: 573704-41-3
C₁₁H₁₅ClN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 4 h / 3102.97 Torr

2.1: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide; ethanol; water / 2 h

3.1: water; lithium hydroxide / methanol / 0 °C

3.2: pH 4

4.1: hydrogenchloride; water / ethyl acetate / 3 h

4.2: 3 h / Cooling with ice

With hydrogenchloride; water; hydrogen; sodium cyanoborohydride; acetic acid; lithium hydroxide; palladium 10% on activated carbon; In methanol; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;