2-Morpholinoethyl-4,5-dichloro-3(2H)-pyridazinone hydrochloride

Base Information

• Chemical Name: 2-Morpholinoethyl-4,5-dichloro-3(2H)-pyridazinone hydrochloride
• CAS No.: 65225-82-3
• Molecular Formula: C10H14Cl3N3O2
• Molecular Weight: 314.599
• DSSTox Substance ID: DTXSID70215528

Synonyms:2-Morpholinoethyl-4,5-dichloro-3(2H)-pyridazinone hydrochloride;65225-82-3;3(2H)-Pyridazinone, 4,5-dichloro-2-(2-(4-morpholinyl)ethyl)-, monohydrochloride;4,5-Dichloro-2-(2-(4-morpholinyl)ethyl)-3(2H)-pyridazinone monohydrochloride;C10H13Cl2N3O2.ClH;SCHEMBL5103337;DTXSID70215528;C10-H13-Cl2-N3-O2.Cl-H;LS-129852

Chemical Property of 2-Morpholinoethyl-4,5-dichloro-3(2H)-pyridazinone hydrochloride

Chemical Property:

• Vapor Pressure: 2.36E-05mmHg at 25°C
• Boiling Point: 359.6°Cat760mmHg
• Flash Point: 171.3°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 313.015160
• Heavy Atom Count: 18
• Complexity: 365

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COCCN1CCN2C(=O)C(=C(C=N2)Cl)Cl.Cl

Technology Process of 2-Morpholinoethyl-4,5-dichloro-3(2H)-pyridazinone hydrochloride

There total 1 articles about 2-Morpholinoethyl-4,5-dichloro-3(2H)-pyridazinone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,5-dichloro-2H-pyridazin-3-one (932-22-9) + 4-(2-chloroethyl)morpholine hydrochride (3647-69-6) → 4,5-dichloro-2-(2-morpholin-4-yl-ethyl)-2H-pyridazin-3-one; hydrochloride (65225-82-3)

Guidance literature:

With sodium ethanolate; In ethanol; dichloromethane; at 80 ℃; for 1h;

Reference yield:

5,5'-dinitro-2,2'-disulfanediyl-bis-aniline (51657-41-1) + 4,5-dichloro-2-(2-morpholin-4-yl-ethyl)-2H-pyridazin-3-one; hydrochloride (65225-82-3) → 5-(2-amino-4-nitro-phenylsulfanyl)-4-chloro-2-(2-morpholin-4-yl-ethyl)-2H-pyridazin-3-one (68434-30-0)

Guidance literature:

Multistep reaction; (i) NaOH, aq. EtOH, (ii) /BRN= 4047392/, KOH, EtOH;

Reference yield:

4,5-dichloro-2-(2-morpholin-4-yl-ethyl)-2H-pyridazin-3-one; hydrochloride (65225-82-3) + 6-nitrobenzo[d]thiazole (2942-06-5) → 5-(2-amino-5-nitro-phenylsulfanyl)-4-chloro-2-(2-morpholin-4-yl-ethyl)-2H-pyridazin-3-one (65225-74-3)

Guidance literature:

Multistep reaction; (i) N₂H₄*H₂O, EtOH, (ii) /BRN= 4047392/, aq. NaOH;

upstream raw materials:

4,5-dichloro-2H-pyridazin-3-one

4-(2-chloroethyl)morpholine hydrochride

Downstream raw materials:

5-(2-amino-4-nitro-phenylsulfanyl)-4-chloro-2-(2-morpholin-4-yl-ethyl)-2H-pyridazin-3-one

5-(2-amino-5-nitro-phenylsulfanyl)-4-chloro-2-(2-morpholin-4-yl-ethyl)-2H-pyridazin-3-one

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