1-[(4-methylphenyl)amino]cyclopentanecarbonitrile

Base Information

• Chemical Name: 1-[(4-methylphenyl)amino]cyclopentanecarbonitrile
• CAS No.: 6636-88-0
• Molecular Formula: C13H16 N2
• Molecular Weight: 200.283

Synonyms:Cyclopentanecarbonitrile,1-p-toluidino- (8CI); 1-[(4-Methylphenyl)amino]cyclopentanecarbonitrile; NSC52316

Chemical Property of 1-[(4-methylphenyl)amino]cyclopentanecarbonitrile

Chemical Property:

• Vapor Pressure: 1.27E-05mmHg at 25°C
• Boiling Point: 368.4°Cat760mmHg
• Flash Point: 176.6°C
• Density: 1.06g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[(4-methylphenyl)amino]cyclopentanecarbonitrile

There total 4 articles about 1-[(4-methylphenyl)amino]cyclopentanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

trimethylsilyl cyanide (7677-24-9) + p-toluidine (106-49-0,12221-03-3) + cyclopentanone (120-92-3) → 1-(4-methylphenyl)aminocyclopentanecarbonitrile (6636-88-0)

Guidance literature:

at 20 ℃; for 6h;

Reference yield: 80.0%

p-toluidine (106-49-0,12221-03-3) + cyclopentanone (120-92-3) + potassium ferrocyanide → 1-(4-methylphenyl)aminocyclopentanecarbonitrile (6636-88-0)

Guidance literature:

potassium ferrocyanide; With benzoyl chloride; at 80 - 160 ℃; for 2h;

p-toluidine; cyclopentanone; In decaethylene glycol; at 80 ℃; for 8h;

DOI:10.1016/j.jorganchem.2012.02.005

Reference yield:

potassium cyanide (151-50-8) + p-toluidine (106-49-0,12221-03-3) + cyclopentanone (120-92-3) → 1-(4-methylphenyl)aminocyclopentanecarbonitrile (6636-88-0)

Guidance literature:

In acetic acid;

upstream raw materials:

potassium cyanide

p-toluidine

cyclopentanone

trimethylsilyl cyanide

Downstream raw materials:

4-Imino-3-phenyl-1-p-tolyl-1,3-diaza-spiro[4.4]nonan-2-one

1-p-toluidino-cyclopentanecarboxylic acid amide

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