4-Allyl-3-hydroxy-2-naphthalenecarboxylic acid methyl ester

Base Information

Chemical Name:4-Allyl-3-hydroxy-2-naphthalenecarboxylic acid methyl ester
CAS No.:57518-88-4
Molecular Formula:C15H14O3
Molecular Weight:242.27000
Hs Code.:
Mol file:57518-88-4.mol

Synonyms:Methyl 4-allyl-3-hydroxy-2-naphthoate;4-Allyl-3-hydroxy-2-naphthalenecarboxylic acid methyl ester;

Suppliers and Price of 4-Allyl-3-hydroxy-2-naphthalenecarboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4-Allyl-3-hydroxy-2-naphthalenecarboxylic acid methyl ester

Chemical Property:

Melting Point:60 °C
Boiling Point:162-164 °C(Press: 0.4 Torr)
PKA:9.26±0.50(Predicted)
PSA：46.53000
Density:1.185±0.06 g/cm3(Predicted)
LogP:3.06050

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Allyl-3-hydroxy-2-naphthalenecarboxylic acid methyl ester

There total 3 articles about 4-Allyl-3-hydroxy-2-naphthalenecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 883-99-8
3-hydroxy-2-naphthoic acid methyl ester

: 106-95-6
allyl bromide

: 57518-88-4
methyl 4-allyl-3-hydroxy-2-naphthoate

Guidance literature:: With sodium hydroxide; acetone; Erhitzen des Reaktionsprodukts unter vermindertem Druck;
DOI:10.1021/jo01220a006 DOI:10.1021/ja01252a511

Reference yield:

: 65550-20-1
methyl 3-allyloxy-2-naphthoate

: 57518-88-4
methyl 4-allyl-3-hydroxy-2-naphthoate

Guidance literature:: at 180 - 190 ℃; under 5 - 7 Torr;

Reference yield:

: 883-99-8
3-hydroxy-2-naphthoic acid methyl ester

: 57518-88-4
methyl 4-allyl-3-hydroxy-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 40percent aq NaOH / acetone / Heating

2: 180 - 190 °C / 5 - 7 Torr

With sodium hydroxide; In acetone;