1,2-Dihydro-2-methylnaphtho[2,1-b]furan-4-carboxylic acid methyl ester

Base Information

Chemical Name:1,2-Dihydro-2-methylnaphtho[2,1-b]furan-4-carboxylic acid methyl ester
CAS No.:67818-27-3
Molecular Formula:C₁₅H₁₄O₃
Molecular Weight:242.274
Hs Code.:
Mol file:67818-27-3.mol

Synonyms:1,2-Dihydro-2-methylnaphtho[2,1-b]furan-4-carboxylic acid methyl ester

Suppliers and Price of 1,2-Dihydro-2-methylnaphtho[2,1-b]furan-4-carboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 1,2-Dihydro-2-methylnaphtho[2,1-b]furan-4-carboxylic acid methyl ester

Chemical Property:

Melting Point:103.5 °C (methanol)
PSA：35.53000
LogP:2.94980

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1,2-Dihydro-2-methylnaphtho[2,1-b]furan-4-carboxylic acid methyl ester

There total 4 articles about 1,2-Dihydro-2-methylnaphtho[2,1-b]furan-4-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57518-88-4
methyl 4-allyl-3-hydroxy-2-naphthoate

: 67818-27-3
2-methyl-1,2-dihydronaphtho(2,1-b)furanocarboxylic-4-acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrochloride / 0.08 h / 260 °C

2: H₂SO₄ / 1 h / Heating

With sulfuric acid; pyridine hydrochloride;

Reference yield:

: 883-99-8
3-hydroxy-2-naphthoic acid methyl ester

: 67818-27-3
2-methyl-1,2-dihydronaphtho(2,1-b)furanocarboxylic-4-acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / 40percent aq NaOH / acetone / Heating

2: 180 - 190 °C / 5 - 7 Torr

3: pyridine hydrochloride / 0.08 h / 260 °C

4: H₂SO₄ / 1 h / Heating

With sodium hydroxide; sulfuric acid; pyridine hydrochloride; In acetone;

Reference yield:

: 65550-20-1
methyl 3-allyloxy-2-naphthoate

: 67818-27-3
2-methyl-1,2-dihydronaphtho(2,1-b)furanocarboxylic-4-acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 180 - 190 °C / 5 - 7 Torr

2: pyridine hydrochloride / 0.08 h / 260 °C

3: H₂SO₄ / 1 h / Heating

With sulfuric acid; pyridine hydrochloride;