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2-Naphthalenecarboxylic acid, 7-ethynyl-3-hydroxy-, hexyl ester

Base Information
  • Chemical Name:2-Naphthalenecarboxylic acid, 7-ethynyl-3-hydroxy-, hexyl ester
  • CAS No.:577040-07-4
  • Molecular Formula:C19H20O3
  • Molecular Weight:296.366
  • Hs Code.:
2-Naphthalenecarboxylic acid, 7-ethynyl-3-hydroxy-, hexyl ester

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Chemical Property of 2-Naphthalenecarboxylic acid, 7-ethynyl-3-hydroxy-, hexyl ester
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Technology Process of 2-Naphthalenecarboxylic acid, 7-ethynyl-3-hydroxy-, hexyl ester

There total 1 articles about 2-Naphthalenecarboxylic acid, 7-ethynyl-3-hydroxy-, hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: 50 percent / H2SO4 / 4 h / 90 °C
2: 95 percent / triethylamine; CuI; PPh3 / PdCl2 / 70 °C
3: 90 percent / TBAF / tetrahydrofuran / 0.5 h / 20 °C
With copper(l) iodide; sulfuric acid; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; palladium dichloride; In tetrahydrofuran;
DOI:10.1021/jo070636+
upstream raw materials:

7-bromo-3-hydroxy-2-naphthoic acid

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