alpha-((1-Naphthalenyloxy)methyl)-4-morpholineethanol

Base Information

• Chemical Name: alpha-((1-Naphthalenyloxy)methyl)-4-morpholineethanol
• CAS No.: 41510-06-9
• Molecular Formula: C17H21NO3
• Molecular Weight: 287.3535
• NSC Number: 89457
• Nikkaji Number: J348.382G
• ChEMBL ID: CHEMBL1906639

Synonyms:NSC89457;41510-06-9;alpha-((1-Naphthalenyloxy)methyl)-4-morpholineethanol;MLS002694946;NSC 89457;BRN 0246740;NSC-89457;4-Morpholineethanol, alpha-((1-naphthalenyloxy)methyl)-;BAS 01507605;Oprea1_021486;Oprea1_229027;4-27-00-00191 (Beilstein Handbook Reference);CHEMBL1906639;SCHEMBL11542140;CGTJUMFMARLZOY-UHFFFAOYSA-N;HMS1675B21;HMS3092C17;AKOS000506778;AKOS016328020;NCI60_041990;SMR001560860;1-(4-morpholinyl)-3-(1-naphthyloxy)-2-propanol;SR-01000313202;SR-01000313202-1;1-Morpholin-4-yl-3-(naphthalen-1-yloxy)propan-2-ol

Chemical Property of alpha-((1-Naphthalenyloxy)methyl)-4-morpholineethanol

Chemical Property:

• Vapor Pressure: 1.74E-10mmHg at 25°C
• Boiling Point: 491.7°Cat760mmHg
• Flash Point: 251.2°C
• Density: 1.182g/cm³
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 287.15214353
• Heavy Atom Count: 21
• Complexity: 306

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COCCN1CC(COC2=CC=CC3=CC=CC=C32)O

Technology Process of alpha-((1-Naphthalenyloxy)methyl)-4-morpholineethanol

There total 3 articles about alpha-((1-Naphthalenyloxy)methyl)-4-morpholineethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

morpholine (110-91-8,99108-56-2) + 3-(1-naphthyloxy)-1,2-epoxypropane (2461-42-9) → dl-N-3-(1-Naphthoxy)-2-hydroxypropylmorpholine (41510-06-9)

Guidance literature:

With cerium(III) chloride heptahydrate; glycerol; at 20 ℃; for 0.816667h; regioselective reaction;

DOI:10.1055/s-0030-1258366

Reference yield:

α-naphthol (90-15-3) → dl-N-3-(1-Naphthoxy)-2-hydroxypropylmorpholine (41510-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH / H₂O

2: 70 percent / ethanol / 6 h / 20 °C

With sodium hydroxide; In ethanol; water;

DOI:10.1007/BF00758612

Reference yield:

→ dl-N-3-(1-Naphthoxy)-2-hydroxypropylmorpholine (41510-06-9)

Guidance literature:

/BRN= 384387/;

DOI:10.1021/ja01617a083

upstream raw materials:

morpholine

3-(1-naphthyloxy)-1,2-epoxypropane

α-naphthol

Downstream raw materials:

4-Allyl-4-[2-hydroxy-3-(naphthalen-1-yloxy)-propyl]-morpholin-4-ium; bromide

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