Technology Process of 4-Pentenimidoyl chloride, 2,2-difluoro-N-(4-methoxyphenyl)-
There total 1 articles about 4-Pentenimidoyl chloride, 2,2-difluoro-N-(4-methoxyphenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2,2-difluoropent-4-enoic acid;
With
tetrachloromethane; triethylamine; triphenylphosphine;
for 0.25h;
Cooling with ice;
Inert atmosphere;
4-methoxy-aniline;
In
tetrachloromethane;
for 3h;
Reflux;
Inert atmosphere;
DOI:10.1002/chem.200702009
- Guidance literature:
-
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride;
In
toluene;
at 95 ℃;
for 15h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1021/jo900296d
- Guidance literature:
-
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride;
In
toluene;
at 95 ℃;
for 96h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1021/jo900296d
