2-CHLOROPHENYL CYCLOHEXYL KETONE

Base Information

• Chemical Name: 2-CHLOROPHENYL CYCLOHEXYL KETONE
• CAS No.: 58139-10-9
• Molecular Formula: C13H15ClO
• Molecular Weight: 222.715
• Hs Code.: 2914700090
• Mol file: 58139-10-9.mol

Synonyms:(2-chlorophenyl)(cyclohexyl)methanone;2-chlorophenyl cyclohexyl ketone;

Chemical Property of 2-CHLOROPHENYL CYCLOHEXYL KETONE

Chemical Property:

• Vapor Pressure: 0.000906mmHg at 25°C
• Boiling Point: 303.9oC at 760 mmHg
• Flash Point: 174oC
• PSA: 17.07000
• Density: 1.139g/cm3
• LogP: 4.10300

Purity/Quality:

95% ^*data from raw suppliers

2-CHLOROPHENYLCYCLOHEXYLKETONE ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLOROPHENYL CYCLOHEXYL KETONE

There total 6 articles about 2-CHLOROPHENYL CYCLOHEXYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-(2-chlorophenyl)cyclohexanecarbaldehyde (1268102-42-6) → (2-chlorophenyl)(cyclohexyl)methanone (58139-10-9)

Guidance literature:

With ferric(III) bromide; In toluene; at 130 ℃; for 14h; chemoselective reaction; Sealed tube; Schlenk technique; Inert atmosphere;

DOI:10.1021/ja4068707

Reference yield: 93.0%

2-Chlorobenzonitrile (873-32-5) + cyclohexylmagnesium bromide (931-50-0) → (2-chlorophenyl)(cyclohexyl)methanone (58139-10-9)

Guidance literature:

With copper(l) iodide; In toluene; for 4h; Reagent/catalyst; Solvent; Inert atmosphere; Reflux;

DOI:10.1007/s11164-014-1790-7

Reference yield: 59.0%

2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) + cyclohexanylcarbonyl chloride (2719-27-9) → (2-chlorophenyl)(cyclohexyl)methanone (58139-10-9)

Guidance literature:

With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; at 0 ℃; for 33.5h;

DOI:10.1039/b701581j

upstream raw materials:

2-(trimethylsilyl)phenyl trifluoromethanesulfonate

cyclohexanylcarbonyl chloride

1-(2-chlorophenyl)cyclohexanecarbaldehyde

2-Chlorophenylacetonitrile

Downstream raw materials:

α-(2-chlorophenyl)-α-cyclohexyl-2-pyridinemethanol

α-(2-Chlorophenyl)-α-cyclohexyl-4-pyridinemethanol

α-(2-chlorophenyl)-α-cyclohexyl-2-pyridinemethane

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