1-(1-Chloro-2,2-difluoroethenyl)-2,3,4,5,6-pentafluorobenzene

Base Information

• Chemical Name: 1-(1-Chloro-2,2-difluoroethenyl)-2,3,4,5,6-pentafluorobenzene
• CAS No.: 58161-50-5
• Molecular Formula: C8ClF7
• Molecular Weight: 264.53
• DSSTox Substance ID: DTXSID90507376
• Mol file: 58161-50-5.mol

Synonyms:58161-50-5;1-(1-Chloro-2,2-difluoroethenyl)-2,3,4,5,6-pentafluorobenzene;alpha-chloroheptafluorostyrene;DTXSID90507376

Chemical Property of 1-(1-Chloro-2,2-difluoroethenyl)-2,3,4,5,6-pentafluorobenzene

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 1
• Exact Mass: 263.9576748
• Heavy Atom Count: 16
• Complexity: 274

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1(=C(C(=C(C(=C1F)F)F)F)F)C(=C(F)F)Cl

Technology Process of 1-(1-Chloro-2,2-difluoroethenyl)-2,3,4,5,6-pentafluorobenzene

There total 19 articles about 1-(1-Chloro-2,2-difluoroethenyl)-2,3,4,5,6-pentafluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

α,α-dichlorodecafluoroisopropylbenzene (179531-49-8) → 1-chloro-2,3,4,5,6-pentafluorobenzene (344-07-0) + α-chloroheptafluorostyrene (58161-50-5)

Guidance literature:

at 620 ℃;

DOI:10.1007/BF00697041

Reference yield: 56.0%

α,α-dichlorodecafluoroisopropylbenzene (179531-49-8) → α-chloroheptafluorostyrene (58161-50-5)

Guidance literature:

With polytetrafluoroethylene; at 470 ℃;

DOI:10.1007/BF00697041

Reference yield: 38.0%

(1,1-dichloro-2,2,2-trifluoroethyl)pentafluorobenzene (5122-18-9) → α-hydro-α-chlorooctafluoroethylbenzene (5122-06-5) + 2,3,4,5,6-pentafluoro-(2,2-difluoroethenyl)benzene (653-19-0) + (2,2,2-trifluoroethyl)pentafluorobenzene (27059-24-1) + α-chloroheptafluorostyrene (58161-50-5)

Guidance literature:

With hydrogenchloride; zinc; In water; N,N-dimethyl-formamide; at 50 ℃; for 5h;

upstream raw materials:

Chlorotrifluoroethylene

1,2,3,4,5-pentafluoro-6-(trichloromethyl)benzene

Chlorodifluoromethane

(1,1-dichloro-2,2,2-trifluoroethyl)pentafluorobenzene

Downstream raw materials:

α,α,β-trichloroperfluoroethylbenzene