6-Methyl-1,3-benzodioxole-5-carbaldehyde

Base Information

Chemical Name:6-Methyl-1,3-benzodioxole-5-carbaldehyde
CAS No.:58343-54-7
Molecular Formula:C9H8O3
Molecular Weight:164.15800
Hs Code.:2932999099
DSSTox Substance ID:DTXSID90389836
Nikkaji Number:J2.312.051H
Wikidata:Q82186033
Mol file:58343-54-7.mol

Synonyms:6-methyl-1,3-benzodioxole-5-carbaldehyde;58343-54-7;6-Methyl-benzo[1,3]dioxole-5-carbaldehyde;6-methyl-2H-1,3-benzodioxole-5-carbaldehyde;6-Methylbenzo[d][1,3]dioxole-5-carbaldehyde;(6-methyl-1,3-benzodioxol-5-yl)carboxaldehyde;SCHEMBL4594814;DTXSID90389836;XEVMQFARCBZBRP-UHFFFAOYSA-N;MFCD04041885;STK394284;AKOS000111504;BS-38210;2-methyl-4,5-(methylenedioxy)benzaldehyde;CS-0315808;FT-0732708;(6-methyl-1,3-benzodioxol-5-yl) carboxaldehyde;(6-methyl-1,3-benzodioxol-5-yl)-carboxaldehyde;6-Methyl-1,3-benzodioxole-5-carbaldehyde, AldrichCPR;F9995-2701

Suppliers and Price of 6-Methyl-1,3-benzodioxole-5-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6-Methyl-1,3-benzodioxole-5-carbaldehyde
500mg
$ 110.00

TRC
6-Methyl-1,3-benzodioxole-5-carbaldehyde
100mg
$ 60.00

TRC
6-Methyl-1,3-benzodioxole-5-carbaldehyde
50mg
$ 45.00

SynQuest Laboratories
6-Methyl-1,3-benzodioxole-5-carbaldehyde 95%
250 mg
$ 208.00

SynQuest Laboratories
6-Methyl-1,3-benzodioxole-5-carbaldehyde 95%
1 g
$ 440.00

Sigma-Aldrich
6-Methyl-1,3-benzodioxole-5-carbaldehyde Aldrich
1g
$ 201.00

Matrix Scientific
6-Methyl-benzo[1,3]dioxole-5-carbaldehyde
1g
$ 378.00

Crysdot
6-Methylbenzo[d][1,3]dioxole-5-carbaldehyde 95+%
5g
$ 539.00

ChemBridge Corporation
6-methyl-1,3-benzodioxole-5-carbaldehyde 95%
5 g
$ 205.00

Apolloscientific
6-Methyl-1,3-benzodioxole-5-carbaldehyde 95%
1g
$ 275.00

Total 4 raw suppliers

Chemical Property of 6-Methyl-1,3-benzodioxole-5-carbaldehyde

Chemical Property:

Vapor Pressure:0.00306mmHg at 25°C
Melting Point:85-88 °C
Boiling Point:284oC at 760 mmHg
Flash Point:116.3oC
PSA：35.53000
Density:1.276g/cm3
LogP:1.53620
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:164.047344113
Heavy Atom Count:12
Complexity:181

Purity/Quality:

97% ^*data from raw suppliers

6-Methyl-1,3-benzodioxole-5-carbaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 52

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1C=O)OCO2

Technology Process of 6-Methyl-1,3-benzodioxole-5-carbaldehyde

There total 3 articles about 6-Methyl-1,3-benzodioxole-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5025-53-6
5-bromo-6-methylbenzo[d][1,3]dioxole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 58343-54-7
(6-methyl-1,3-benzodioxol-5-yl)carboxaldehyde

Guidance literature:: 5-bromo-6-methylbenzo[d][1,3]dioxole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 ℃; for 1.16667h;

With water; In tetrahydrofuran; hexane;

Reference yield: 96.0%

: 7145-99-5
5-methyl-1,3-benzodioxole

: 4885-02-3
Dichloromethyl methyl ether

: 58343-54-7
(6-methyl-1,3-benzodioxol-5-yl)carboxaldehyde

Guidance literature:: 5-methyl-1,3-benzodioxole; Dichloromethyl methyl ether; In dichloromethane; at 0 ℃;

With titanium tetrachloride; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2006.02.015