Benzene, 1-[[[(2S,3E)-4-iodo-2-methyl-3-butenyl]oxy]methyl]-4-methoxy-

Base Information

Chemical Name:Benzene, 1-[[[(2S,3E)-4-iodo-2-methyl-3-butenyl]oxy]methyl]-4-methoxy-
CAS No.:583866-35-7
Molecular Formula:C13H17IO2
Molecular Weight:332.181
Hs Code.:

Synonyms:

Suppliers and Price of Benzene, 1-[[[(2S,3E)-4-iodo-2-methyl-3-butenyl]oxy]methyl]-4-methoxy-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-[[[(2S,3E)-4-iodo-2-methyl-3-butenyl]oxy]methyl]-4-methoxy-

Chemical Property:

Purity/Quality:

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Technology Process of Benzene, 1-[[[(2S,3E)-4-iodo-2-methyl-3-butenyl]oxy]methyl]-4-methoxy-

There total 3 articles about Benzene, 1-[[[(2S,3E)-4-iodo-2-methyl-3-butenyl]oxy]methyl]-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 583866-35-7
p-methoxybenzyl (2S,3E)-4-iodo-2-methyl-3-butenyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 9.6 g / triflic acid / CH₂Cl₂; petroleum ether / 0.5 h / 20 °C

2: diisobutylaluminum hydride / diethyl ether; hexane / 1.5 h / -78 °C

3: 322 mg / chromium(II) chloride / tetrahydrofuran; dioxane / 5 h / 0 - 20 °C

With chromium dichloride; trifluorormethanesulfonic acid; diisobutylaluminium hydride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; dichloromethane; Petroleum ether;
DOI:10.1021/jo0301301

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 583866-35-7
p-methoxybenzyl (2S,3E)-4-iodo-2-methyl-3-butenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / diethyl ether

2: 9.6 g / triflic acid / CH₂Cl₂; petroleum ether / 0.5 h / 20 °C

3: diisobutylaluminum hydride / diethyl ether; hexane / 1.5 h / -78 °C

4: 322 mg / chromium(II) chloride / tetrahydrofuran; dioxane / 5 h / 0 - 20 °C

With chromium dichloride; trifluorormethanesulfonic acid; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; dichloromethane; Petroleum ether;
DOI:10.1021/jo0301301

Reference yield:

: 212051-35-9
(R)-methyl 3-((4-methoxybenzyl)oxy)-2-methylpropanoate

: 583866-35-7
p-methoxybenzyl (2S,3E)-4-iodo-2-methyl-3-butenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminum hydride / diethyl ether; hexane / 1.5 h / -78 °C

2: 322 mg / chromium(II) chloride / tetrahydrofuran; dioxane / 5 h / 0 - 20 °C

With chromium dichloride; diisobutylaluminium hydride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane;
DOI:10.1021/jo0301301