Benzene, 1-(bromomethyl)-3-methoxy-2-(phenylmethoxy)-

Base Information

Chemical Name:Benzene, 1-(bromomethyl)-3-methoxy-2-(phenylmethoxy)-
CAS No.:58402-40-7
Molecular Formula:C15H15BrO2
Molecular Weight:307.187
Hs Code.:
DSSTox Substance ID:DTXSID70445868
Wikidata:Q82264409

Synonyms:58402-40-7;Benzene, 1-(bromomethyl)-3-methoxy-2-(phenylmethoxy)-;SCHEMBL9802381;DTXSID70445868;AYNKAXMSZZZOKZ-UHFFFAOYSA-N;2-Benzyloxy-3-bromomethyl-1-methoxybenzene

Suppliers and Price of Benzene, 1-(bromomethyl)-3-methoxy-2-(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Benzene, 1-(bromomethyl)-3-methoxy-2-(phenylmethoxy)-

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:306.02554
Heavy Atom Count:18
Complexity:229

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1OCC2=CC=CC=C2)CBr

Technology Process of Benzene, 1-(bromomethyl)-3-methoxy-2-(phenylmethoxy)-

There total 6 articles about Benzene, 1-(bromomethyl)-3-methoxy-2-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.2%

: 52508-44-8
2-benzyloxy-3-hydroxymethyl-1-methoxybenzene

: 58402-40-7
2-(benzyloxy)-3-(bromomethyl)-1-methoxybenzene

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.ejmech.2013.06.016

Reference yield: 65.0%

: 52508-44-8
2-benzyloxy-3-hydroxymethyl-1-methoxybenzene

: 7789-60-8
phosphorus tribromide

: 58402-40-7
2-(benzyloxy)-3-(bromomethyl)-1-methoxybenzene

Guidance literature:: In diethyl ether;

Reference yield:

: 2011-06-5
2-benzyloxy-3-methoxybenzaldehyde

: 58402-40-7
2-(benzyloxy)-3-(bromomethyl)-1-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / 1 h / 0 - 20 °C

2: phosphorus tribromide / 1,4-dioxane / 1 h / 40 °C

With sodium tetrahydroborate; phosphorus tribromide; In 1,4-dioxane;
DOI:10.1021/jo400737f