Silane, (1,1-dimethylethyl)dimethyl[2-[5-(phenylmethoxy)-2-cyclopenten-1-yl]eth oxy]-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)dimethyl[2-[5-(phenylmethoxy)-2-cyclopenten-1-yl]eth oxy]-
CAS No.:587875-05-6
Molecular Formula:C20H32O2Si
Molecular Weight:332.558
Hs Code.:

Synonyms:

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Chemical Property of Silane, (1,1-dimethylethyl)dimethyl[2-[5-(phenylmethoxy)-2-cyclopenten-1-yl]eth oxy]-

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Technology Process of Silane, (1,1-dimethylethyl)dimethyl[2-[5-(phenylmethoxy)-2-cyclopenten-1-yl]eth oxy]-

There total 4 articles about Silane, (1,1-dimethylethyl)dimethyl[2-[5-(phenylmethoxy)-2-cyclopenten-1-yl]eth oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 587875-04-5
2-(5-benzyloxy-cyclopent-2-enyl)-ethanol

: 587875-05-6
[2-(5-benzyloxy-cyclopent-2-enyl)-ethoxy]-tert-butyl-dimethyl-silane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
DOI:10.1016/S0957-4166(03)00452-X

Reference yield:

: 587875-02-3
2-(2-Hydroxy-ethyl)-cyclopent-3-enol

: 587875-05-6
[2-(5-benzyloxy-cyclopent-2-enyl)-ethoxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 53 percent / pTsOH / CH₂Cl₂ / 2.5 h / 20 °C

2: NaH / dimethylformamide / 0 - 20 °C

3: 750 mg / aq. H₂SO₄ / acetonitrile / 27 h / 20 °C

4: 84 percent / imidazole / dimethylformamide / 20 h / 20 °C

With 1H-imidazole; sulfuric acid; sodium hydride; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0957-4166(03)00452-X

Reference yield:

: 587875-03-4
2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopent-3-enol

: 587875-05-6
[2-(5-benzyloxy-cyclopent-2-enyl)-ethoxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide / 0 - 20 °C

2: 750 mg / aq. H₂SO₄ / acetonitrile / 27 h / 20 °C

3: 84 percent / imidazole / dimethylformamide / 20 h / 20 °C

With 1H-imidazole; sulfuric acid; sodium hydride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0957-4166(03)00452-X