Dabigatran Impurity 22

Base Information

Chemical Name:Dabigatran Impurity 22
CAS No.:58906-62-0
Molecular Formula:C7H13ClO2
Molecular Weight:164.63000
Hs Code.:
Mol file:58906-62-0.mol

Synonyms:chlorocarbonic acid-(1-ethyl-butyl ester);Chlorameisensaeure-(aethylpropylcarbin)-ester;3-hexyl chloroformate;Chlorokohlensaeure-(1-aethyl-butylester);

Suppliers and Price of Dabigatran Impurity 22

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-HexylChloroformate(>80%)
5g
$ 810.00

AK Scientific
Hexan-3-ylcarbonochloridate
1g
$ 1342.00

Total 23 raw suppliers

Chemical Property of Dabigatran Impurity 22

Chemical Property:

PSA：26.30000
LogP:2.94050
Storage Temp.:Hygroscopic, Refrigerator, under inert atmosphere
Solubility.:Chloroform (Slightly), Ethyl Acetate (Slightly)

Purity/Quality:

98% ^*data from raw suppliers

3-HexylChloroformate(>80%) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 3-Hexyl Chloroformate is a potential impurity in the synthesis of Dabigatran Etexilate Mesylate (D100150); a nonpeptide and direct thrombin inhibitor. Antithrombotic.

Technology Process of Dabigatran Impurity 22

There total 2 articles about Dabigatran Impurity 22 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-44-5
phosgene

: 623-37-0
n-hexan-3-ol

: 58906-62-0
hexan-3-yl chloroformate

Guidance literature:: With nitrogen; In benzene;

Reference yield:

: 623-37-0
n-hexan-3-ol

: 32315-10-9
bis(trichloromethyl) carbonate

: 58906-62-0
hexan-3-yl chloroformate

Guidance literature:: bis(trichloromethyl) carbonate; With potassium carbonate; N,N-dimethyl-formamide; In toluene; at 0 ℃; for 1h;

n-hexan-3-ol; In toluene; for 5h;
DOI:10.1021/op500084q