Silane, [2-(2-bromo-2-cyclohexen-1-yl)-1-(5-methyl-2-furanyl)ethoxy](1,1-dimeth ylethyl)dimethyl-

Base Information

Chemical Name:Silane, [2-(2-bromo-2-cyclohexen-1-yl)-1-(5-methyl-2-furanyl)ethoxy](1,1-dimeth ylethyl)dimethyl-
CAS No.:591727-31-0
Molecular Formula:C₁₉H₃₁BrO₂Si
Molecular Weight:399.443
Hs Code.:

Synonyms:

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Chemical Property of Silane, [2-(2-bromo-2-cyclohexen-1-yl)-1-(5-methyl-2-furanyl)ethoxy](1,1-dimeth ylethyl)dimethyl-

Chemical Property:

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Technology Process of Silane, [2-(2-bromo-2-cyclohexen-1-yl)-1-(5-methyl-2-furanyl)ethoxy](1,1-dimeth ylethyl)dimethyl-

There total 5 articles about Silane, [2-(2-bromo-2-cyclohexen-1-yl)-1-(5-methyl-2-furanyl)ethoxy](1,1-dimeth ylethyl)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 534-22-5
2-methylfuran

: 591727-31-0
[2-(2-bromocyclohex-2-enyl)-1-(5-methylfuran-2-yl)ethoxy]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: nBuLi / hexane; tetrahydrofuran / 2 h / -78 °C

1.2: 70 percent / tetrahydrofuran; hexane / 3 h / 20 °C

2.1: 75 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -25 °C

With 2,6-dimethylpyridine; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.200210329

Reference yield:

: 17202-32-3
1,6-dibromocyclohex-1-ene

: 591727-31-0
[2-(2-bromocyclohex-2-enyl)-1-(5-methylfuran-2-yl)ethoxy]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1.1: 53 percent / nBuLi; iso-propylcyclohexylamine / 1,2-dimethoxy-ethane

2.1: 80 percent / lithium aluminum hydride / diethyl ether / 20 °C

3.1: 82 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h

4.1: nBuLi / hexane; tetrahydrofuran / 2 h / -78 °C

4.2: 70 percent / tetrahydrofuran; hexane / 3 h / 20 °C

5.1: 75 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -25 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; n-butyllithium; N-cyclohexylisopropylamine; Dess-Martin periodane; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane;
DOI:10.1002/ejoc.200210329

Reference yield:

: 591727-29-6
(2-bromocyclohex-2-enyl)acetaldehyde

: 591727-31-0
[2-(2-bromocyclohex-2-enyl)-1-(5-methylfuran-2-yl)ethoxy]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: nBuLi / hexane; tetrahydrofuran / 2 h / -78 °C

1.2: 70 percent / tetrahydrofuran; hexane / 3 h / 20 °C

2.1: 75 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -25 °C

With 2,6-dimethylpyridine; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.200210329