2,2'-methylenebis[3-chlorotoluene]

Base Information

Chemical Name:2,2'-methylenebis[3-chlorotoluene]
CAS No.:84604-92-2
Molecular Formula:C15H14 Cl2
Molecular Weight:265.182
Hs Code.:2903999090
Mol file:84604-92-2.mol

Synonyms:2,2’-methylenebis[3-chlorotoluene]

Suppliers and Price of 2,2'-methylenebis[3-chlorotoluene]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 2,2'-methylenebis[3-chlorotoluene]

Chemical Property:

Boiling Point:362.2oC at 760 mmHg
Flash Point:160.9oC
PSA：0.00000
Density:1.177g/cm3
LogP:5.20100

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2'-methylenebis[3-chlorotoluene]

There total 4 articles about 2,2'-methylenebis[3-chlorotoluene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 134271-35-5
bis(2-chloro-6-methylphenyl)methanol

: 84604-92-2
bis(2-chloro-6-methylphenyl)methane

Guidance literature:: With dimethylsilicon dichloride; sodium iodide; In acetonitrile; for 20.5h;
DOI:10.1016/0022-328X(91)86224-E

Reference yield:

: 87-63-8
2-chloro-6-methylaniline

: 84604-92-2
bis(2-chloro-6-methylphenyl)methane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, conc. HCl, 2.) sodium acetate, sodium sulfite / 1.) water, 10 deg C, 60 min, 2.) from 10 to 15 deg C, 2 h

2: 1.) n-BuLi / 1.) hexane, THF, ether, -95 deg C, 30 min, 2.) from -95 deg C to RT, overnight

3: 69 percent / dichlorodimethylsilane, NaI / acetonitrile / 20.5 h

With hydrogenchloride; n-butyllithium; sodium acetate; dimethylsilicon dichloride; sodium iodide; sodium sulfite; sodium nitrite; In acetonitrile;
DOI:10.1016/0022-328X(91)86224-E

Reference yield:

: 69190-56-3
2-bromo-1-chloro-3-methylbenzene

: 84604-92-2
bis(2-chloro-6-methylphenyl)methane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) hexane, THF, ether, -95 deg C, 30 min, 2.) from -95 deg C to RT, overnight

2: 69 percent / dichlorodimethylsilane, NaI / acetonitrile / 20.5 h

With n-butyllithium; dimethylsilicon dichloride; sodium iodide; In acetonitrile;
DOI:10.1016/0022-328X(91)86224-E