Tellurocyanic acid, 2-oxo-2-phenylethyl ester

Base Information

• Chemical Name: Tellurocyanic acid, 2-oxo-2-phenylethyl ester
• CAS No.: 592511-88-1
• Molecular Formula: C9H7NOTe
• Molecular Weight: 272.761
• Mol file: 592511-88-1.mol

Synonyms:

Chemical Property of Tellurocyanic acid, 2-oxo-2-phenylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tellurocyanic acid, 2-oxo-2-phenylethyl ester

There total 1 articles about Tellurocyanic acid, 2-oxo-2-phenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

potassium cyanide (151-50-8) + α-bromoacetophenone (70-11-1) → phenacyl tellurocyanate (592511-88-1)

Guidance literature:

potassium cyanide; With tellurium; In dimethyl sulfoxide; for 1h; Heating;

α-bromoacetophenone; In dimethyl sulfoxide; at 20 ℃; for 2h;

DOI:10.1016/S0022-328X(03)00152-9

Reference yield: 90.0%

phenacyl tellurocyanate (592511-88-1) → C8H7Cl3OTe

Guidance literature:

With thionyl chloride; In diethyl ether;

DOI:10.1016/S0022-328X(03)00152-9

Reference yield: 84.0%

phenacyl tellurocyanate (592511-88-1) → C8H7I3OTe

Guidance literature:

With iodine; In diethyl ether; at 20 ℃;

DOI:10.1016/S0022-328X(03)00152-9

upstream raw materials:

potassium cyanide

α-bromoacetophenone

Downstream raw materials:

diphenacyl ditelluride

dichloro-diphenacyl-λ⁴-tellane

diphenacyl telluride

diphenacyltellurium diiodide