Naphthalene, 1,2-dihydro-8-phenyl-

Base Information

Chemical Name:Naphthalene, 1,2-dihydro-8-phenyl-
CAS No.:592549-18-3
Molecular Formula:C16H14
Molecular Weight:206.287
Hs Code.:

Synonyms:

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Chemical Property of Naphthalene, 1,2-dihydro-8-phenyl-

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Technology Process of Naphthalene, 1,2-dihydro-8-phenyl-

There total 8 articles about Naphthalene, 1,2-dihydro-8-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 910330-44-8
5-phenyl-1-tetralol

: 592549-18-3
8-phenyl-1,2-dihydronaphthalene

Guidance literature:: With oxalic acid; In water; for 5h; Heating;
DOI:10.1016/j.bmc.2006.05.077

Reference yield:

: 123206-83-7
4-(2-Bromophenyl)-1-butanol

: 592549-18-3
8-phenyl-1,2-dihydronaphthalene

Guidance literature:: Multi-step reaction with 6 steps

1: 58 percent / chromium trioxide; acetic acid / 18 h / 20 °C

2: thionyl chloride / 0.75 h / Heating

3: 540 mg / aluminium chloride / CS₂ / 3 h / Heating

4: 86 percent / Na₂CO₃ / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene; ethanol / 24 h / Heating

5: 90 percent / NaBH₄ / toluene; methanol; H₂O / 1 h / 20 °C

6: 74 percent / oxalic acid / H₂O / 5 h / Heating

With chromium(VI) oxide; sodium tetrahydroborate; aluminium trichloride; thionyl chloride; oxalic acid; sodium carbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; carbon disulfide; ethanol; water; toluene; 4: Suzuki-Miyaura cross-coupling;
DOI:10.1016/j.bmc.2006.05.077

Reference yield:

: 90841-47-7
4-(2-bromophenyl)butanoic acid

: 592549-18-3
8-phenyl-1,2-dihydronaphthalene

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 0.75 h / Heating

2: 540 mg / aluminium chloride / CS₂ / 3 h / Heating

3: 86 percent / Na₂CO₃ / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene; ethanol / 24 h / Heating

4: 90 percent / NaBH₄ / toluene; methanol; H₂O / 1 h / 20 °C

5: 74 percent / oxalic acid / H₂O / 5 h / Heating

With sodium tetrahydroborate; aluminium trichloride; thionyl chloride; oxalic acid; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; carbon disulfide; ethanol; water; toluene; 3: Suzuki-Miyaura cross-coupling;
DOI:10.1016/j.bmc.2006.05.077