5-phenyl-1-tetralol

Base Information

Chemical Name:5-phenyl-1-tetralol
CAS No.:910330-44-8
Molecular Formula:C₁₆H₁₆O
Molecular Weight:224.302
Hs Code.:

Synonyms:5-phenyl-1-tetralol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-phenyl-1-tetralol

Chemical Property:

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Technology Process of 5-phenyl-1-tetralol

There total 7 articles about 5-phenyl-1-tetralol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 90401-62-0
5-phenyl-1-tetralone

: 910330-44-8
5-phenyl-1-tetralol

Guidance literature:: With sodium tetrahydroborate; In methanol; water; toluene; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2006.05.077

Reference yield:

: 123206-83-7
4-(2-Bromophenyl)-1-butanol

: 910330-44-8
5-phenyl-1-tetralol

Guidance literature:: Multi-step reaction with 5 steps

1: 58 percent / chromium trioxide; acetic acid / 18 h / 20 °C

2: thionyl chloride / 0.75 h / Heating

3: 540 mg / aluminium chloride / CS₂ / 3 h / Heating

4: 86 percent / Na₂CO₃ / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene; ethanol / 24 h / Heating

5: 90 percent / NaBH₄ / toluene; methanol; H₂O / 1 h / 20 °C

With chromium(VI) oxide; sodium tetrahydroborate; aluminium trichloride; thionyl chloride; sodium carbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; carbon disulfide; ethanol; water; toluene; 4: Suzuki-Miyaura cross-coupling;
DOI:10.1016/j.bmc.2006.05.077

Reference yield:

: 90841-47-7
4-(2-bromophenyl)butanoic acid

: 910330-44-8
5-phenyl-1-tetralol

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 0.75 h / Heating

2: 540 mg / aluminium chloride / CS₂ / 3 h / Heating

3: 86 percent / Na₂CO₃ / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene; ethanol / 24 h / Heating

4: 90 percent / NaBH₄ / toluene; methanol; H₂O / 1 h / 20 °C

With sodium tetrahydroborate; aluminium trichloride; thionyl chloride; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; carbon disulfide; ethanol; water; toluene; 3: Suzuki-Miyaura cross-coupling;
DOI:10.1016/j.bmc.2006.05.077