Butanoic acid, 3-phenoxy-, (3S)-

Base Information

Chemical Name:Butanoic acid, 3-phenoxy-, (3S)-
CAS No.:594836-78-9
Molecular Formula:C10H12O3
Molecular Weight:180.203
Hs Code.:

Synonyms:

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Chemical Property of Butanoic acid, 3-phenoxy-, (3S)-

Chemical Property:

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Technology Process of Butanoic acid, 3-phenoxy-, (3S)-

There total 5 articles about Butanoic acid, 3-phenoxy-, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (E)-3-phenoxybut-2-enoic acid

: 594836-78-9
(S)-3-phenoxybutanoic acid

Guidance literature:: (E)-3-phenoxybut-2-enoic acid; With morpholine; In dichloromethane; water; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; C₂₄H₂₁O₃P; P(p-CH₃OC₆H₄)3; In dichloromethane; water; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

With hydrogen; In diethyl ether; dichloromethane; at 20 ℃; for 16h; under 19001.3 Torr; enantioselective reaction; Autoclave; Glovebox;
DOI:10.1002/chem.201503229

Reference yield: 84.0%

: 594836-74-5
(S)-butyl 3-phenoxybutanoate

: 594836-78-9
(S)-3-phenoxybutanoic acid

Guidance literature:: With Pseudomonas cepacia Amano PS lipase; In phosphate buffer; at 20 ℃; for 23h; pH=7;
DOI:10.1016/S0957-4166(03)00277-5

Reference yield:

: 64508-87-8
3-phenoxybutanoic acid

: 594836-78-9
(S)-3-phenoxybutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / Na₂SO₄; Burkholderia cepacia lipase Chirazyme(R) L-1 / hexane / 12 h / 20 °C

2: 84 percent / Pseudomonas cepacia Amano PS lipase / aq. phosphate buffer / 23 h / 20 °C / pH 7

With Pseudomonas cepacia Amano PS lipase; Burkholderia cepacia lipase Chirazyme(R) L-1; sodium sulfate; In phosphate buffer; hexane;
DOI:10.1016/S0957-4166(03)00277-5