BenzeneMethanol, 3-Methyl-.alpha.-(trichloroMethyl)-

Base Information

• Chemical Name: BenzeneMethanol, 3-Methyl-.alpha.-(trichloroMethyl)-
• CAS No.: 59881-69-5
• Molecular Formula: C9H9Cl3O
• Molecular Weight: 239.52600
• Mol file: 59881-69-5.mol

Synonyms:BENZENEMETHANOL,3-METHYL-.ALPHA.-(TRICHLOROMETHYL)-;2,2,2-Trichlor-1-m-tolyl-aethanol;2,2,2-trichloro-1-m-tolyl-ethanol;2,2,2-TRICHLORO-1-M-TOLYLETHANOL;

Chemical Property of BenzeneMethanol, 3-Methyl-.alpha.-(trichloroMethyl)-

Chemical Property:

• PSA: 20.23000
• LogP: 3.39860

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BenzeneMethanol, 3-Methyl-.alpha.-(trichloroMethyl)-

There total 2 articles about BenzeneMethanol, 3-Methyl-.alpha.-(trichloroMethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

chloroform (67-66-3,8013-54-5) + m-tolyl aldehyde (620-23-5) → (+/-)-2,2,2-trichloro-1-(3-methylphenyl)ethanol (59881-69-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 20 ℃; for 12h;

DOI:10.1021/jo8007644

Reference yield:

m-tolyl aldehyde (620-23-5) → (+/-)-2,2,2-trichloro-1-(3-methylphenyl)ethanol (59881-69-5)

Guidance literature:

With potassium hydroxide; chloroform;

DOI:10.1021/ja01167a051

Reference yield: 96.0%

(+/-)-2,2,2-trichloro-1-(3-methylphenyl)ethanol (59881-69-5) → 3-methylphenyl chloromethyl ketone (21886-54-4)

Guidance literature:

With [2,2]bipyridinyl; copper(l) chloride; In 1,2-dichloro-ethane; for 3h; Heating;

DOI:10.1021/jo8007644

upstream raw materials:

m-tolyl aldehyde

chloroform

Downstream raw materials:

2,2,2-trichloro-1-(3-methylphenyl)ethanone

(R)-2,2,2-trichloro-1-(3-methylphenyl)ethanol

3-methylphenyl chloromethyl ketone

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