11-Diethylaminomethyl-9,10-dihydro-9,10-ethanoanthracene

Base Information

• Chemical Name: 11-Diethylaminomethyl-9,10-dihydro-9,10-ethanoanthracene
• CAS No.: 14692-45-6
• Molecular Formula: C₂₁H₂₅N
• Molecular Weight: 291.436
• Hs Code.: 2921499090
• DSSTox Substance ID: DTXSID30932961
• Nikkaji Number: J49.811D
• Mol file: 14692-45-6.mol

Synonyms:14692-45-6;BRN 2386764;11-Diethylaminomethyl-9,10-dihydro-9,10-ethanoanthracene;11-(Diethylaminomethyl)-9,10-dihydro-9,10-ethanoanthracene;9,10-Dihydro-11-diethylaminomethyl-9,10-ethanoanthracene;9,10-Ethanoanthracene, 9,10-dihydro-11-(diethylaminomethyl)-;N-ethyl-N-(15-tetracyclo[6.6.2.02,7.09,14]hexadeca-2,4,6,9,11,13-hexaenylmethyl)ethanamine;DTXSID30932961;LS-66294;9,10-Ethanoanthracene-11-methylamine, N,N-diethyl-9,10-dihydro-;N-[(9,10-Dihydro-9,10-ethanoanthracen-11-yl)methyl]-N-ethylethanamine

Chemical Property of 11-Diethylaminomethyl-9,10-dihydro-9,10-ethanoanthracene

Chemical Property:

• Vapor Pressure: 8.88E-07mmHg at 25°C
• Melting Point: 78 °C
• Boiling Point: 405.3°Cat760mmHg
• PKA: 10.16±0.25(Predicted)
• Flash Point: 177.5°C
• PSA: 3.24000
• Density: 1.052g/cm³
• LogP: 4.62550
• XLogP3: 4.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 291.198699802
• Heavy Atom Count: 22
• Complexity: 350

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)CC1CC2C3=CC=CC=C3C1C4=CC=CC=C24

Technology Process of 11-Diethylaminomethyl-9,10-dihydro-9,10-ethanoanthracene

There total 2 articles about 11-Diethylaminomethyl-9,10-dihydro-9,10-ethanoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibenzobicyclo[2.2.2]octa-2,5-diene-7-carbaldehyde (7673-68-9) + diethylamine (109-89-7) → 11-Diaethylaminomethyl-9.10-dihydro-9.10-aethano-anthracen (14692-45-6)

Guidance literature:

With formic acid; In benzene;

DOI:10.1021/jm00313a018

Reference yield:

→ 11-Diaethylaminomethyl-9.10-dihydro-9.10-aethano-anthracen (14692-45-6)

Guidance literature:

Entspr. Carbonsaeure, 1)SOCl2, 2)Et2NH, 3)LiAlH4;

upstream raw materials:

dibenzobicyclo[2.2.2]octa-2,5-diene-7-carbaldehyde

diethylamine

Refernces