3,4-Bis(benzyloxy)-6,7-dihydro-5H-benzo[7]annulene

Base Information

Chemical Name:3,4-Bis(benzyloxy)-6,7-dihydro-5H-benzo[7]annulene
CAS No.:60055-03-0
Molecular Formula:C₂₅H₂₄O₂
Molecular Weight:356.464
Hs Code.:
DSSTox Substance ID:DTXSID30574249

Synonyms:60055-03-0;3,4-Bis(benzyloxy)-6,7-dihydro-5H-benzo[7]annulene;DTXSID30574249

Suppliers and Price of 3,4-Bis(benzyloxy)-6,7-dihydro-5H-benzo[7]annulene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3,4-Bis(benzyloxy)-6,7-dihydro-5H-benzo[7]annulene

Chemical Property:

XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:356.177630004
Heavy Atom Count:27
Complexity:447

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC=CC2=C(C1)C(=C(C=C2)OCC3=CC=CC=C3)OCC4=CC=CC=C4

Technology Process of 3,4-Bis(benzyloxy)-6,7-dihydro-5H-benzo[7]annulene

There total 4 articles about 3,4-Bis(benzyloxy)-6,7-dihydro-5H-benzo[7]annulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54131-01-0
1,2-dihydroxy-6,7,8,9-tetrahydro-5H-benzocylohepten-5-one

: 60055-03-0
1,2-Dibenzyloxy-8,9-dihydro-7H-benzocyclo-hepten

Guidance literature:: Multi-step reaction with 3 steps

1: (i) K₂CO₃, KI, Na₂S₂O₃, EtOH, (ii) KOH

2: NaBH₄ / methanol

3: KHSO₄ / benzene

With sodium tetrahydroborate; potassium hydrogensulfate; In methanol; benzene;
DOI:10.1248/cpb.26.504

Reference yield:

: 54130-94-8
2,3-dimethoxy-6,7,8,9-tetrahydro-5H-benzo[a]cyclohepten-5-one

: 60055-03-0
1,2-Dibenzyloxy-8,9-dihydro-7H-benzocyclo-hepten

Guidance literature:: Multi-step reaction with 4 steps

1: AlCl₃ / benzene

2: (i) K₂CO₃, KI, Na₂S₂O₃, EtOH, (ii) KOH

3: NaBH₄ / methanol

4: KHSO₄ / benzene

With sodium tetrahydroborate; potassium hydrogensulfate; aluminium trichloride; In methanol; benzene;
DOI:10.1248/cpb.26.504

Reference yield:

: 60055-00-7
1,2-dibenzyloxy-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

: 60055-03-0
1,2-Dibenzyloxy-8,9-dihydro-7H-benzocyclo-hepten

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol

2: KHSO₄ / benzene

With sodium tetrahydroborate; potassium hydrogensulfate; In methanol; benzene;
DOI:10.1248/cpb.26.504