2H-Pyrrole, 3,4-dihydro-2-methyl-2-(methylphenylphosphinyl)-, 1-oxide

Base Information

Chemical Name:2H-Pyrrole, 3,4-dihydro-2-methyl-2-(methylphenylphosphinyl)-, 1-oxide
CAS No.:600738-65-6
Molecular Formula:C₁₂H₁₆NO₂P
Molecular Weight:237.238
Hs Code.:
DSSTox Substance ID:DTXSID80475994
Nikkaji Number:J1.914.461E

Synonyms:600738-65-6;2H-Pyrrole, 3,4-dihydro-2-methyl-2-(methylphenylphosphinyl)-, 1-oxide;DTXSID80475994

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-Pyrrole, 3,4-dihydro-2-methyl-2-(methylphenylphosphinyl)-, 1-oxide

Chemical Property:

XLogP3:0.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:237.09186575
Heavy Atom Count:16
Complexity:347

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CCC=[N+]1[O-])P(=O)(C)C2=CC=CC=C2

Technology Process of 2H-Pyrrole, 3,4-dihydro-2-methyl-2-(methylphenylphosphinyl)-, 1-oxide

There total 4 articles about 2H-Pyrrole, 3,4-dihydro-2-methyl-2-(methylphenylphosphinyl)-, 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 600738-64-5
2-methyl-2-(methyl-phenyl-phosphinoyl)-pyrrolidine

: 600738-65-6
2-(methylphenylphosphoryl)-2-methyl-3,4-dihydro-2H-pyrroline N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at -10 ℃;
DOI:10.1246/cl.2003.604

Reference yield:

: 5891-21-4
5-chloro-2-pentanone

: 600738-65-6
2-(methylphenylphosphoryl)-2-methyl-3,4-dihydro-2H-pyrroline N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / ethanol / 50 °C

2: m-CPBA / CHCl₃ / -10 °C

With ammonia; 3-chloro-benzenecarboperoxoic acid; In ethanol; chloroform;
DOI:10.1246/cl.2003.604

Reference yield:

: 19315-13-0,102222-19-5,102222-20-8,891848-03-6
methyl(phenyl)phosphineoxide

: 600738-65-6
2-(methylphenylphosphoryl)-2-methyl-3,4-dihydro-2H-pyrroline N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / ethanol / 50 °C

2: m-CPBA / CHCl₃ / -10 °C

With ammonia; 3-chloro-benzenecarboperoxoic acid; In ethanol; chloroform;
DOI:10.1246/cl.2003.604