3-Hydroxy-5-methylbenzaldehyde

Base Information

Chemical Name:3-Hydroxy-5-methylbenzaldehyde
CAS No.:60549-26-0
Molecular Formula:C8H8O2
Molecular Weight:136.15
Hs Code.:2912499000
DSSTox Substance ID:DTXSID10485187
Wikidata:Q82324146
Mol file:60549-26-0.mol

Synonyms:3-Hydroxy-5-methylbenzaldehyde;60549-26-0;Benzaldehyde, 3-hydroxy-5-methyl-;5-hydroxy-m-tolualdehyde;SCHEMBL1619002;DTXSID10485187;BTLHCFVCIGAAPF-UHFFFAOYSA-N;CL9235;MFCD16999707;AKOS016007413;AB71633;DS-16766;CS-0153252;A868949

Suppliers and Price of 3-Hydroxy-5-methylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemcia Scientific
3-Hydroxy-5-methyl-benzaldehyde 95%
1 G
$ 150.00

AOBChem
3-Hydroxy-5-methylbenzaldehyde 97%
1g
$ 108.00

AOBChem
3-Hydroxy-5-methylbenzaldehyde 97%
5g
$ 385.00

American Custom Chemicals Corporation
3-HYDROXY-5-METHYLBENZALDEHYDE 95.00%
5MG
$ 500.08

Ambeed
3-Hydroxy-5-methylbenzaldehyde 98%
1g
$ 128.00

Ambeed
3-Hydroxy-5-methylbenzaldehyde 98%
250mg
$ 54.00

Ambeed
3-Hydroxy-5-methylbenzaldehyde 98%
100mg
$ 33.00

Ambeed
3-Hydroxy-5-methylbenzaldehyde 98%
5g
$ 467.00

Alichem
3-Hydroxy-5-methylbenzaldehyde
500mg
$ 980.00

Alichem
3-Hydroxy-5-methylbenzaldehyde
1g
$ 1685.00

Total 15 raw suppliers

Chemical Property of 3-Hydroxy-5-methylbenzaldehyde

Chemical Property:

Melting Point:107-108 °C(Solv: chloroform (67-66-3))
Boiling Point:259.2±20.0 °C(Predicted)
PKA:9.35±0.10(Predicted)
PSA：37.30000
Density:1.175±0.06 g/cm3(Predicted)
LogP:1.51310
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:136.052429494
Heavy Atom Count:10
Complexity:122

Purity/Quality:

97% ^*data from raw suppliers

3-Hydroxy-5-methyl-benzaldehyde 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)O)C=O

Technology Process of 3-Hydroxy-5-methylbenzaldehyde

There total 4 articles about 3-Hydroxy-5-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 90003-09-1
2-Chloro-5-methylcyclohex-1-en-1-carbaldehyd

: 60549-26-0
3-hydroxy-5-methylbenzaldehyde

Guidance literature:: With oxygen; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 20h;

Reference yield: 60.0%

: 90674-26-3
3-methoxy-5-methyl-benzaldehyde

: 60549-26-0
3-hydroxy-5-methylbenzaldehyde

Guidance literature:: 3-methoxy-5-methyl-benzaldehyde; With boron tribromide; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; acetic acid; In dichloromethane; water; for 10h; Reflux; Inert atmosphere;
DOI:10.1021/ja305113d

Reference yield:

: 119650-44-1
(3-methoxy-5-methylphenyl)methanol

: 60549-26-0
3-hydroxy-5-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: silica gel; pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

2.1: boron tribromide / dichloromethane / 2 h / 20 °C / Inert atmosphere

2.2: 10 h / Reflux; Inert atmosphere

With silica gel; boron tribromide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/ja305113d