2-Pyridinecarboxylic acid, 5-(phenylmethyl)-, methyl ester

Base Information

Chemical Name:2-Pyridinecarboxylic acid, 5-(phenylmethyl)-, methyl ester
CAS No.:60611-82-7
Molecular Formula:C14H13NO2
Molecular Weight:227.263
Hs Code.:

Synonyms:

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Chemical Property of 2-Pyridinecarboxylic acid, 5-(phenylmethyl)-, methyl ester

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Technology Process of 2-Pyridinecarboxylic acid, 5-(phenylmethyl)-, methyl ester

There total 4 articles about 2-Pyridinecarboxylic acid, 5-(phenylmethyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 957065-99-5
5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine-2-carboxylic acid methyl ester

: 60611-82-7
methyl 5-benzylpicolinate

Guidance literature:: With caesium carbonate; In 1,4-dioxane; water; at 110 ℃; for 0.5h; Sealed tube; Microwave irradiation;
DOI:10.1016/j.ejmech.2016.11.044

Reference yield:

: 29682-15-3
methyl 5-bromopicolinate

: 60611-82-7
methyl 5-benzylpicolinate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 0.25 h / 110 °C / Sealed tube; Microwave irradiation

2: caesium carbonate / 1,4-dioxane; water / 0.5 h / 110 °C / Sealed tube; Microwave irradiation

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; caesium carbonate; In 1,4-dioxane; water; 2: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2016.11.044

Reference yield:

: 624-28-2
2,5-dibromopyridine

: 60611-82-7
methyl 5-benzylpicolinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilylmethyllithium / toluene / 0.5 h / -78 - 0 °C

1.2: 3 h

1.3: 18 h / 20 °C

2.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 0.25 h / 110 °C / Sealed tube; Microwave irradiation

3.1: caesium carbonate / 1,4-dioxane; water / 0.5 h / 110 °C / Sealed tube; Microwave irradiation

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; trimethylsilylmethyllithium; caesium carbonate; In 1,4-dioxane; water; toluene; 3.1: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2016.11.044