Phenol, 2,4,6-tris(1,1-dimethylethyl)-, lithium salt

Base Information

Chemical Name:Phenol, 2,4,6-tris(1,1-dimethylethyl)-, lithium salt
CAS No.:60693-39-2
Molecular Formula:C18H30O.Li
Molecular Weight:268.369
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 2,4,6-tris(1,1-dimethylethyl)-, lithium salt

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Phenol, 2,4,6-tris(1,1-dimethylethyl)-, lithium salt

There total 1 articles about Phenol, 2,4,6-tris(1,1-dimethylethyl)-, lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 732-26-3
2,4,6-tri-tert-butylphenoxol

: 60693-39-2
lithium 2,4,6-tri-tert-butylphenolate

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 0.5h;
DOI:10.1021/ja00526a053

Reference yield: 90.0%

: 13597-22-3
tantalum oxytrichloride

: 60693-39-2
lithium 2,4,6-tri-tert-butylphenolate

: 159277-80-2
tris(2,4,6-tri-tert-butylphenoxo)-oxotantalum(V)

Guidance literature:: In diethyl ether; prepn. under Ar; addn. of Li-compd. to a suspn. of TaOCl3 in Et2O at room temp. with stirring, further stirring for 24 h; centrifugation, evapn. of solvent under vac., drying at 35°C under vac., elem. anal.;

Reference yield: 65.0%

: 60693-39-2
lithium 2,4,6-tri-tert-butylphenolate

: 80545-62-6
tert-butylimidovanadium(V) trichloride

: Dichloro-2,4,6-tri-tert-butylphenolato-tert-butylimidovanadium(V)

Guidance literature:: In toluene; byproducts: LiCl; under Ar, -78 °C, V-compd:Li-compd. molar ratio was 1:1, stirring for 3 h at room temp.; ppt. was centrifuged, extd. twice with toluene, combined solns. was evapd. in vac., residue was recrystd. from n-hexane with use of dry ice, elem. anal.;