Piperazine, 1-(2-iodobenzoyl)-4-methyl-

Base Information

Chemical Name:Piperazine, 1-(2-iodobenzoyl)-4-methyl-
CAS No.:60787-03-3
Molecular Formula:C₁₂H₁₅IN₂O
Molecular Weight:330.168
Hs Code.:
DSSTox Substance ID:DTXSID30388702
Wikidata:Q82183836

Synonyms:Piperazine, 1-(2-iodobenzoyl)-4-methyl-;60787-03-3;(2-iodophenyl)-(4-methylpiperazin-1-yl)methanone;1-(2-iodobenzoyl)-4-methylpiperazine;Oprea1_068897;DTXSID30388702;AKOS003945115;AE-641/30108021

Suppliers and Price of Piperazine, 1-(2-iodobenzoyl)-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Piperazine, 1-(2-iodobenzoyl)-4-methyl-

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:330.02291
Heavy Atom Count:16
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCN(CC1)C(=O)C2=CC=CC=C2I

Technology Process of Piperazine, 1-(2-iodobenzoyl)-4-methyl-

There total 4 articles about Piperazine, 1-(2-iodobenzoyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-01-3
1-methyl-piperazine

: 88-67-5
2-Iodobenzoic acid

: 60787-03-3
1-(2-iodobenzoyl)-4-methylpiperazine

Guidance literature:: 2-Iodobenzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;

1-methyl-piperazine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/acs.joc.8b02682

Reference yield:

: 109-01-3
1-methyl-piperazine

: 60787-03-3
1-(2-iodobenzoyl)-4-methylpiperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / CHCl₃ / 1)stirred 1h,room temp. 2)reflux 1h

2: aqueous NH₃

With ammonium hydroxide; In chloroform;

Reference yield:

: 609-67-6
2-Iodobenzoyl chloride

: 60787-03-3
1-(2-iodobenzoyl)-4-methylpiperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / CHCl₃ / 1)stirred 1h,room temp. 2)reflux 1h

2: aqueous NH₃

With ammonium hydroxide; In chloroform;