1H-1,5-Benzodiazepine-2,4(3H,5H)-dione, 3-ethyl-3-(2-propenyl)-

Base Information

Chemical Name:1H-1,5-Benzodiazepine-2,4(3H,5H)-dione, 3-ethyl-3-(2-propenyl)-
CAS No.:54871-36-2
Molecular Formula:C14H16N2O2
Molecular Weight:244.289
Hs Code.:
DSSTox Substance ID:DTXSID60203358
Wikidata:Q83076734

Synonyms:BRN 0794884;1H-1,5-Benzodiazepine-2,4(3H,5H)-dione, 3-ethyl-3-(2-propenyl)-;3-Ethyl-3-(2-propenyl)-1H-1,5-benzodiazepine-2,4(3H,5H)-dione;5-24-08-00228 (Beilstein Handbook Reference);54871-36-2;DTXSID60203358;LS-34110

Suppliers and Price of 1H-1,5-Benzodiazepine-2,4(3H,5H)-dione, 3-ethyl-3-(2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-1,5-Benzodiazepine-2,4(3H,5H)-dione, 3-ethyl-3-(2-propenyl)-

Chemical Property:

Vapor Pressure:1.97E-08mmHg at 25°C
Boiling Point:454.1°Cat760mmHg
Flash Point:182.3°C
Density:1.089g/cm³
XLogP3:2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:244.121177757
Heavy Atom Count:18
Complexity:339

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1(C(=O)NC2=CC=CC=C2NC1=O)CC=C

Technology Process of 1H-1,5-Benzodiazepine-2,4(3H,5H)-dione, 3-ethyl-3-(2-propenyl)-

There total 1 articles about 1H-1,5-Benzodiazepine-2,4(3H,5H)-dione, 3-ethyl-3-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54871-36-2
3-allyl-3-ethyl-1,5-dihydro-benzo[b][1,4]diazepine-2,4-dione

Guidance literature:: o-Phenylendiamin, Ethylallylmalonat, EtONa, in Toluol;

Reference yield: 90.0%

: 54871-36-2
3-allyl-3-ethyl-1,5-dihydro-benzo[b][1,4]diazepine-2,4-dione

: 77420-13-4
10a-Ethyl-2-methyl-1,2,9,10a-tetrahydro-3-oxa-4,9-diaza-benzo[f]azulen-10-one

Guidance literature:: With sulfuric acid; for 0.5h; Ambient temperature;

Reference yield:

: 54871-36-2
3-allyl-3-ethyl-1,5-dihydro-benzo[b][1,4]diazepine-2,4-dione

: 77414-12-1
10a-Ethyl-2-methyl-1,2,3a,4,9,10a-hexahydro-3-oxa-4,9-diaza-benzo[f]azulen-10-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 100percent H₂SO₄ / 0.5 h / Ambient temperature

2: 81 percent / NaBH₄ / methanol / 2 h / Ambient temperature

With sodium tetrahydroborate; sulfuric acid; In methanol;