9-Acridinamine, 1,2,3,4-tetrahydro-N-butyl-7-chloro-

Base Information

Chemical Name:9-Acridinamine, 1,2,3,4-tetrahydro-N-butyl-7-chloro-
CAS No.:34811-16-0
Molecular Formula:C17H21ClN2
Molecular Weight:288.815
Hs Code.:
DSSTox Substance ID:DTXSID40188351
Wikidata:Q83060156

Synonyms:BRN 0412420;9-ACRIDINAMINE, 1,2,3,4-TETRAHYDRO-N-BUTYL-7-CHLORO-;1,2,3,4-Tetrahydro-N-butyl-7-chloro-9-acridinamine;34811-16-0;C17H21ClN2;DTXSID40188351

Suppliers and Price of 9-Acridinamine, 1,2,3,4-tetrahydro-N-butyl-7-chloro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Acridinamine, 1,2,3,4-tetrahydro-N-butyl-7-chloro-

Chemical Property:

Vapor Pressure:1.62E-08mmHg at 25°C
Boiling Point:456.4°Cat760mmHg
Flash Point:229.8°C
Density:1.181g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:288.1393264
Heavy Atom Count:20
Complexity:309

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCNC1=C2CCCCC2=NC3=C1C=C(C=C3)Cl

Technology Process of 9-Acridinamine, 1,2,3,4-tetrahydro-N-butyl-7-chloro-

There total 4 articles about 9-Acridinamine, 1,2,3,4-tetrahydro-N-butyl-7-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1629174-85-1
7-chloro-1,2,3,4-tetrahydroacridin-9-yl trifluoromethanesulfonate

: 109-73-9,85404-21-3
N-butylamine

: 34811-16-0
7-chloro-9-n-butylamino-1,2,3,4-tetrahydroacridine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; at 130 ℃; for 1h; Microwave irradiation; Inert atmosphere;
DOI:10.1002/ejoc.201402122

Reference yield: 67.0%

: 53618-66-9
4,6-Dichloro-2,3-tetramethylenequinoline

: 109-73-9,85404-21-3
N-butylamine

: 34811-16-0
7-chloro-9-n-butylamino-1,2,3,4-tetrahydroacridine

Guidance literature:: With phenol; at 125 - 130 ℃; for 3h;

Reference yield:

: 113106-05-1,643757-30-6
7-chloro-1,2,3 ,4-tetrahydroacridin-9-(10H)-one

: 34811-16-0
7-chloro-9-n-butylamino-1,2,3,4-tetrahydroacridine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 17 h / -78 - 20 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / 1,4-dioxane / 1 h / 130 °C / Microwave irradiation; Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; In 1,4-dioxane; dichloromethane; 2: |Buchwald-Hartwig Coupling;
DOI:10.1002/ejoc.201402122