1-Cyclohexyl-3-methyl-1-butanone

Base Information

Chemical Name:1-Cyclohexyl-3-methyl-1-butanone
CAS No.:62106-65-4
Molecular Formula:C11H20O
Molecular Weight:168.279
Hs Code.:
European Community (EC) Number:663-323-1
DSSTox Substance ID:DTXSID40399869
Nikkaji Number:J1.836.799H
Wikidata:Q82202632

Synonyms:1-Cyclohexyl-3-methyl-1-butanone;62106-65-4;1-Butanone, 1-cyclohexyl-3-methyl-;SCHEMBL5909830;DTXSID40399869;AKOS010016494

Suppliers and Price of 1-Cyclohexyl-3-methyl-1-butanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-Cyclohexyl-3-methyl-1-butanone

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:168.151415257
Heavy Atom Count:12
Complexity:143

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CC(=O)C1CCCCC1

Technology Process of 1-Cyclohexyl-3-methyl-1-butanone

There total 11 articles about 1-Cyclohexyl-3-methyl-1-butanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 503607-15-6
1-cyclohexyl-1-[dimethyl(phenyl)silyl]-3-methylbutan-1-ol

: 62106-65-4
Cyclohexyl 2-methylpropyl ketone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1002/1522-2675(200210)85:10<3349::AID-HLCA3349>3.0.CO;2-K

Reference yield: 32.0%

: 15378-40-2
trans-1-cyclohexyl-2-buten-1-one

: 31729-70-1
bis(iodozinc)methane

: 62106-65-4
Cyclohexyl 2-methylpropyl ketone

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 0.5h;
DOI:10.1055/s-2001-12336

Reference yield:

: 2719-27-9
cyclohexanylcarbonyl chloride

: 62106-65-4
Cyclohexyl 2-methylpropyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran; toluene / 1 h / -78 °C

1.2: 45 percent / toluene; tetrahydrofuran / -78 - 20 °C

2.1: 81 percent / nBu₄NF / tetrahydrofuran / 4 h / 20 °C

3.1: 83 percent / PCC / CH₂Cl₂ / 18 h / 20 °C

With tetrabutyl ammonium fluoride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; toluene; 1.1: Brook rearrangement;
DOI:10.1002/1522-2675(200210)85:10<3349::AID-HLCA3349>3.0.CO;2-K