[2-(Methoxymethoxy)phenyl](diphenyl)phosphane

Base Information

Chemical Name:[2-(Methoxymethoxy)phenyl](diphenyl)phosphane
CAS No.:62815-32-1
Molecular Formula:C20H19O2P
Molecular Weight:322.343
Hs Code.:
DSSTox Substance ID:DTXSID00557660
Nikkaji Number:J2.102.440F
Wikidata:Q82439625

Synonyms:62815-32-1;SCHEMBL14066484;DTXSID00557660;o-methoxymethoxyphenyldiphenylphosphine;(2-(Methoxymethoxy)phenyl)diphenylphosphane;[2-(Methoxymethoxy)phenyl](diphenyl)phosphane

Suppliers and Price of [2-(Methoxymethoxy)phenyl](diphenyl)phosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-(Methoxymethoxy)phenyl](diphenyl)phosphane

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:322.11226684
Heavy Atom Count:23
Complexity:306

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COCOC1=CC=CC=C1P(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of [2-(Methoxymethoxy)phenyl](diphenyl)phosphane

There total 4 articles about [2-(Methoxymethoxy)phenyl](diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 824-91-9
O-methoxymethylphenol

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 62815-32-1
methoxymethyl o-diphenylphosphinophenyl ether

Guidance literature:: O-methoxymethylphenol; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at 20 ℃; for 1.5h;

chloro-diphenylphosphine; In hexane; at 20 ℃; for 16h;
DOI:10.1021/jo060409s

Reference yield:

: 108-95-2,27073-41-2
phenol

: 62815-32-1
methoxymethyl o-diphenylphosphinophenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 74 percent / NaH / dimethylformamide; various solvent(s) / 0 - 20 °C

2.1: n-BuLi; TMEDA / hexane / 1.5 h / 20 °C

2.2: 61 percent / hexane / 16 h / 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; In hexane; N,N-dimethyl-formamide;
DOI:10.1021/jo060409s

Reference yield:

: 108-95-2,27073-41-2
phenol

: 62815-32-1
methoxymethyl o-diphenylphosphinophenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / NaOH, Bu₄NBr / benzene; H₂O / 4 h / Heating

2: 1) butyl lithium

With sodium hydroxide; n-butyllithium; tetrabutylammomium bromide; In water; benzene;
DOI:10.1007/BF00953718