1,1'-(9-Ethyl-9H-carbazole-3,6-diyl)bis(phenylethane-1,2-dione)

Base Information

Chemical Name:1,1'-(9-Ethyl-9H-carbazole-3,6-diyl)bis(phenylethane-1,2-dione)
CAS No.:62913-23-9
Molecular Formula:C30H21NO4
Molecular Weight:459.501
Hs Code.:
DSSTox Substance ID:DTXSID00488642
Wikidata:Q82331436

Synonyms:62913-23-9;DTXSID00488642;1,1'-(9-Ethyl-9H-carbazole-3,6-diyl)bis(phenylethane-1,2-dione);3,6-bis(phenylglyoxalyl)(9-ethyl-9h-carbazole)

Suppliers and Price of 1,1'-(9-Ethyl-9H-carbazole-3,6-diyl)bis(phenylethane-1,2-dione)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,1'-(9-Ethyl-9H-carbazole-3,6-diyl)bis(phenylethane-1,2-dione)

Chemical Property:

PSA：73.21000
LogP:5.94560
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:459.14705815
Heavy Atom Count:35
Complexity:758

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN1C2=C(C=C(C=C2)C(=O)C(=O)C3=CC=CC=C3)C4=C1C=CC(=C4)C(=O)C(=O)C5=CC=CC=C5

Technology Process of 1,1'-(9-Ethyl-9H-carbazole-3,6-diyl)bis(phenylethane-1,2-dione)

There total 6 articles about 1,1'-(9-Ethyl-9H-carbazole-3,6-diyl)bis(phenylethane-1,2-dione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 62913-25-1
9-ethyl-3,6-bis(2-phenylethynyl)-9H-carbazole

: 62913-23-9
2,2'-diphenyl-1,1'-(9-ethyl-carbazole-3,6-diyl)-bis-ethanedione

Guidance literature:: With potassium permanganate; acetic acid; In acetone; Heating;
DOI:10.1134/S0012500807010053

Reference yield: 58.0%

: 1396318-11-8
C₃₀H₂₅N

: 62913-23-9
2,2'-diphenyl-1,1'-(9-ethyl-carbazole-3,6-diyl)-bis-ethanedione

Guidance literature:: With tert.-butylhydroperoxide; [Ru₂Cl(3,6-bis(1-(2-pyridylmethyl)imidazol-2-yliden-3-yl)pyridazine)(CH₃CN)₄](PF₆)₃; sodium iodide; In water; acetonitrile; at 20 ℃; for 0.166667h;
DOI:10.1021/om300644h

Reference yield:

: 33255-13-9
3,6-dibromo-9-ethyl-9H-carbazole

: 62913-23-9
2,2'-diphenyl-1,1'-(9-ethyl-carbazole-3,6-diyl)-bis-ethanedione

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine; PPh₃; CuI / PdCl₂(PPh₃)2 / 10 h / Heating

2: 96 percent / KMnO₄; CH₃COOH / acetone / Heating

With potassium permanganate; copper(l) iodide; acetic acid; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; In acetone;
DOI:10.1134/S0012500807010053