9-Ethyl-3,6-bis(phenylethynyl)-9H-carbazole

Base Information

Chemical Name:9-Ethyl-3,6-bis(phenylethynyl)-9H-carbazole
CAS No.:62913-25-1
Molecular Formula:C30H21N
Molecular Weight:395.503
Hs Code.:
DSSTox Substance ID:DTXSID40488641
Nikkaji Number:J3.640.108G
Wikidata:Q82331434

Synonyms:62913-25-1;9-Ethyl-3,6-bis(phenylethynyl)-9H-carbazole;DTXSID40488641;3,6-bis(phenylethynyl)(9-ethyl-9h-carbazole)

Suppliers and Price of 9-Ethyl-3,6-bis(phenylethynyl)-9H-carbazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Ethyl-3,6-bis(phenylethynyl)-9H-carbazole

Chemical Property:

XLogP3:7.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:395.167399674
Heavy Atom Count:31
Complexity:665

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN1C2=C(C=C(C=C2)C#CC3=CC=CC=C3)C4=C1C=CC(=C4)C#CC5=CC=CC=C5

Technology Process of 9-Ethyl-3,6-bis(phenylethynyl)-9H-carbazole

There total 5 articles about 9-Ethyl-3,6-bis(phenylethynyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 33255-13-9
3,6-dibromo-9-ethyl-9H-carbazole

: 536-74-3
phenylacetylene

: 62913-25-1
9-ethyl-3,6-bis(2-phenylethynyl)-9H-carbazole

Guidance literature:: With copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; for 10h; Heating;
DOI:10.1134/S0012500807010053

Reference yield: 91.0%

: 57103-07-8
9-ethyl-3,6-diiodocarbazole

: 536-74-3
phenylacetylene

: 62913-25-1
9-ethyl-3,6-bis(2-phenylethynyl)-9H-carbazole

Guidance literature:: With copper (I) iodide; triphenylphosphine; palladium on activated charcoal; In diethylamine; at 50 ℃; oth. catalyst (PdCl₂, 75percent);

Reference yield: 72.0%

: 74-96-4
ethyl bromide

: 62913-24-0
3,6-bis(2-phenylethynyl)-9H-carbazole

: 62913-25-1
9-ethyl-3,6-bis(2-phenylethynyl)-9H-carbazole

Guidance literature:: 3,6-bis(2-phenylethynyl)-9H-carbazole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.75h; Inert atmosphere;

ethyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.dyepig.2016.09.062