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2-[4-(methylsulfanyl)phenyl]-3-(pyridin-4-yl)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole

Base Information Edit
  • Chemical Name:2-[4-(methylsulfanyl)phenyl]-3-(pyridin-4-yl)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole
  • CAS No.:122454-68-6
  • Molecular Formula:C18H17 N3 S
  • Molecular Weight:307.4127
  • Hs Code.:
  • Mol file:122454-68-6.mol
2-[4-(methylsulfanyl)phenyl]-3-(pyridin-4-yl)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole

Synonyms:SKF 105561

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 2-[4-(methylsulfanyl)phenyl]-3-(pyridin-4-yl)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole Edit
Chemical Property:
  • Vapor Pressure:5.37E-10mmHg at 25°C 
  • Boiling Point:509.5°Cat760mmHg 
  • Flash Point:262°C 
  • PSA:56.01000 
  • Density:1.26g/cm3 
  • LogP:4.28020 
Purity/Quality:
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MSDS Files:

SDS file from LookChem

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Technology Process of 2-[4-(methylsulfanyl)phenyl]-3-(pyridin-4-yl)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole

There total 8 articles about 2-[4-(methylsulfanyl)phenyl]-3-(pyridin-4-yl)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; for 18h; Ambient temperature;
DOI:10.1016/S0040-4039(00)76529-4
Guidance literature:
Multi-step reaction with 5 steps
1: 75 percent / CHCl3 / 3 h / Ambient temperature
2: 77 percent / H2O / 9 h / Heating
3: 75 percent / CH2Cl2 / Ambient temperature
4: 56 percent / t-BuOK, t-BuOH, O2 / 19 h / Heating
5: 73 percent / dimethylformamide / 18 h / 80 °C
With potassium tert-butylate; oxygen; tert-butyl alcohol; In dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(96)00212-X
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