2-Methyl-4-phenyl-6H-1,3-oxazin-6-one

Base Information

Chemical Name:2-Methyl-4-phenyl-6H-1,3-oxazin-6-one
CAS No.:76569-84-1
Molecular Formula:C11H9 N O2
Molecular Weight:187.1947
Hs Code.:
NSC Number:167379
DSSTox Substance ID:DTXSID60304798
Nikkaji Number:J398.947J
Wikidata:Q82051011

Synonyms:2-Methyl-4-phenyl-6H-1,3-oxazin-6-one;76569-84-1;NSC167379;DTXSID60304798;NSC-167379

Suppliers and Price of 2-Methyl-4-phenyl-6H-1,3-oxazin-6-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-Methyl-4-phenyl-6H-1,3-oxazin-6-one

Chemical Property:

Vapor Pressure:0.000596mmHg at 25°C
Boiling Point:310.6°Cat760mmHg
Flash Point:150.2°C
Density:1.16g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:187.063328530
Heavy Atom Count:14
Complexity:298

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC(=CC(=O)O1)C2=CC=CC=C2

Technology Process of 2-Methyl-4-phenyl-6H-1,3-oxazin-6-one

There total 12 articles about 2-Methyl-4-phenyl-6H-1,3-oxazin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 107465-78-1
N-[(2,2-Dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene)-phenyl-methyl]-acetamide

: 76569-84-1
2-methyl-4-phenyl-6H-1,3-oxazin-6-one

Guidance literature:: In neat (no solvent); at 160 - 165 ℃; for 0.166667h;

Reference yield: 84.0%

: 57957-24-1
N-(1-phenylvinyl)acetamide

: 76569-84-1
2-methyl-4-phenyl-6H-1,3-oxazin-6-one

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; carbon monoxide; copper diacetate; palladium diacetate; acetic anhydride; potassium iodide; In N,N-dimethyl-formamide; at 80 ℃; Reagent/catalyst; Solvent;
DOI:10.1002/anie.201307942

Reference yield: 82.0%

: 201230-82-2
carbon monoxide

: 57957-24-1
N-(1-phenylvinyl)acetamide

: 76569-84-1
2-methyl-4-phenyl-6H-1,3-oxazin-6-one

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; tris(2,2'-bipyridyl)ruthenium dichloride; oxygen; palladium diacetate; acetic anhydride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Reagent/catalyst; Schlenk technique; Irradiation;
DOI:10.1021/acs.joc.6b00965