2-Propenoic acid, 2-Methyl-, 4,4,4-trifluoro-3-hydroxy-1-Methyl-3-(trifluoroMethyl)butyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 2-Methyl-, 4,4,4-trifluoro-3-hydroxy-1-Methyl-3-(trifluoroMethyl)butyl ester
• CAS No.: 630414-85-6
• Molecular Formula: C10H12F6O3
• Molecular Weight: 294.194
• Hs Code.: 2918199890
• Mol file: 630414-85-6.mol

Synonyms:4,4,4-trifluoro-3-hydroxy-1-methyl-3-(trifluoromethyl)butyl 2-methylacrylate;2-PROPENOIC ACID,2-METHYL-,4,4,4-TRIFLUORO-3-HYDROXY-1-METHYL-3-(TRIFLUOROMETHYL)BUTYL ESTER;5,5,5-Trifluoro-4-hydroxy-4-(trifluoromethyl)pentan-2-yl methacrylate;4,4,4-trifluoro-3-hydroxy-1-methyl-3-(trifluoromethyl)butyl 2-methacrylate;FD2105;1,1,1-Trifluoro-2-trifluoromethyl-2-hydroxy-4-pentyl methacrylate;

Chemical Property of 2-Propenoic acid, 2-Methyl-, 4,4,4-trifluoro-3-hydroxy-1-Methyl-3-(trifluoroMethyl)butyl ester

Chemical Property:

• Boiling Point: 291.0±40.0 °C(Predicted)
• PKA: 9.32±0.29(Predicted)
• PSA: 46.53000
• Density: 1.321±0.06 g/cm3(Predicted)
• LogP: 2.74000

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 2-Methyl-, 4,4,4-trifluoro-3-hydroxy-1-Methyl-3-(trifluoroMethyl)butyl ester

There total 5 articles about 2-Propenoic acid, 2-Methyl-, 4,4,4-trifluoro-3-hydroxy-1-Methyl-3-(trifluoroMethyl)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

→ 5,5,5-trifluoro-4-hydroxy-4-(trifluoromethyl)pentan-2-yl methacrylate (630414-85-6)

Guidance literature:

Reference yield: 58.8%

methacryloyl anhydride (760-93-0) + 1,1,1-trifluoro-2-(trifluoromethyl)pentane-2,4-diol (34844-48-9) → 5,5,5-trifluoro-4-hydroxy-4-(trifluoromethyl)pentan-2-yl methacrylate (630414-85-6)

Guidance literature:

With 10H-phenothiazine; methanesulfonic acid; In toluene; at 50 ℃; for 4h; Product distribution / selectivity; Heating / reflux;

Reference yield:

poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) + 1,1,1-trifluoro-2-(trifluoromethyl)pent-4-en-2-ol (646-97-9) → 5,5,5-trifluoro-4-hydroxy-4-(trifluoromethyl)pentan-2-yl methacrylate (630414-85-6) + 2-hydroxy-1,1,1-trifluoro-2-trifluoromethylpentan-3-yl methacrylate

Guidance literature:

tris-(trifluoromethanesulfonyl)methane acid; at 110 ℃; for 7h;

upstream raw materials:

poly(methacrylic acid)

1,1,1-trifluoro-2-(trifluoromethyl)pentane-2,4-diol

methacryloyl anhydride

Methacryloyl chloride

Refernces

• 1、 -. "The fluorine-containing polymerizable monomer distillation purification method". Paragraph 0200; 0201; 0202; 0205; 0207. . Retrieved 2019/05/25.
• 2、 -. "Precursors to fluoroalkanol-containing olefin monomers and associated methods of synthesis and use". Page/Page column 13. . Retrieved 2008/06/13.