2,4,6-TRIPHENYLANILINE

Base Information

• Chemical Name: 2,4,6-TRIPHENYLANILINE
• CAS No.: 6864-20-6
• Molecular Formula: C24H19 N
• Molecular Weight: 321.422
• Hs Code.: 2921499090
• Mol file: 6864-20-6.mol

Synonyms:Aniline,2,4,6-triphenyl- (6CI,7CI); [m-Terphenyl]-2'-amine, 5'-phenyl- (8CI);2,4,6-Triphenylaniline; Benzenamine, 2,4,6-triphenyl-

Chemical Property of 2,4,6-TRIPHENYLANILINE

Chemical Property:

• Vapor Pressure: 7.73E-09mmHg at 25°C
• Melting Point: 122-125 °C(lit.)
• Boiling Point: 465.4°C at 760 mmHg
• Flash Point: 245.5°C
• PSA: 26.02000
• Density: 1.117g/cm³
• LogP: 6.85100

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,4,6-Triphenylaniline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6-TRIPHENYLANILINE

There total 5 articles about 2,4,6-TRIPHENYLANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,4,6-tribromoaniline (147-82-0) + phenylboronic acid (98-80-6) → 2,4,6-triphenylaniline (6864-20-6)

Guidance literature:

With potassium phosphate tribasic heptahydrate; palladium diacetate; In water; N,N-dimethyl-formamide; at 80 ℃; for 0.5h;

DOI:10.3998/ark.5550190.0013.906

Reference yield: 90.0%

2-nitro-1,3,5-triphenyl-benzene (10368-47-5) → 2,4,6-triphenylaniline (6864-20-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In water; isopropyl alcohol; at 80 ℃; for 14h;

DOI:10.1021/ic300870y

Reference yield: 70.0%

4-chloro-2,6-dibromoaniline (874-17-9) + phenylboronic acid (98-80-6) → 2,4,6-triphenylaniline (6864-20-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; Reflux;

upstream raw materials:

2-nitro-1,3,5-triphenyl-benzene

2,4,6-tribromoaniline

phenylboronic acid

1,3,5-triphenylbenzene

Downstream raw materials:

2,4,6-triphenylphenol

N-<(3-nitrophenyl)thio>-2,4,6-triphenylaniline

N-[(4-nitrophenyl)thio]-2,4,6-triphenylaniline

N-<(4-methylphenyl)thio>-2,4,6-triphenylaniline