Technology Process of 7-Octenoic acid, 6-(acetyloxy)-, 6-methoxy-6-oxo-5-(phenylsulfonyl)hexyl
ester
There total 7 articles about 7-Octenoic acid, 6-(acetyloxy)-, 6-methoxy-6-oxo-5-(phenylsulfonyl)hexyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
for 2h;
Heating;
DOI:10.1021/ja00534a030
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 71 percent / tetrahydrofuran / 1 h / 0 °C
2: 91 percent / potassium hydroxide / aq. ethanol / 2.5 h / Ambient temperature
3: 60 percent / pyridine / Ambient temperature
4: thionyl chloride / diethyl ether / 4 h / Ambient temperature
5: 84 percent / pyridine / CH2Cl2 / 2 h / Heating
With
pyridine; potassium hydroxide; thionyl chloride;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/ja00534a030
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 75 percent / pyridinium chlorochromate, sodum acetate / CH2Cl2 / 1 h / Ambient temperature
2: 71 percent / tetrahydrofuran / 1 h / 0 °C
3: 91 percent / potassium hydroxide / aq. ethanol / 2.5 h / Ambient temperature
4: 60 percent / pyridine / Ambient temperature
5: thionyl chloride / diethyl ether / 4 h / Ambient temperature
6: 84 percent / pyridine / CH2Cl2 / 2 h / Heating
With
pyridine; potassium hydroxide; thionyl chloride; sodium acetate; pyridinium chlorochromate;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/ja00534a030
