4-[(E)-(4-Methylpentan-2-ylidene)amino]-N-phenylaniline

Base Information

• Chemical Name: 4-[(E)-(4-Methylpentan-2-ylidene)amino]-N-phenylaniline
• CAS No.: 63302-40-9
• Molecular Formula: C18H22N2
• Molecular Weight: 266.386
• DSSTox Substance ID: DTXSID80556934
• Nikkaji Number: J29.848D
• Mol file: 63302-40-9.mol

Synonyms:63302-40-9;SCHEMBL5078512;4-[(E)-(4-Methylpentan-2-ylidene)amino]-N-phenylaniline;DTXSID80556934

Chemical Property of 4-[(E)-(4-Methylpentan-2-ylidene)amino]-N-phenylaniline

Chemical Property:

• XLogP3: 4.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 266.178298710
• Heavy Atom Count: 20
• Complexity: 295

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)CC(=NC1=CC=C(C=C1)NC2=CC=CC=C2)C

Technology Process of 4-[(E)-(4-Methylpentan-2-ylidene)amino]-N-phenylaniline

There total 2 articles about 4-[(E)-(4-Methylpentan-2-ylidene)amino]-N-phenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-2-pentanone (108-10-1) + N-phenylphenylene-1,4-diamine (101-54-2) → N-(1,3-dimethylbutyl)-N'-phenyl-p-phenylenediamine (793-24-8) + C18H22N2 (63302-40-9)

Guidance literature:

With palladium on activated charcoal; hydrogen; at 200 ℃; under 30003 Torr; Reagent/catalyst;

DOI:10.1039/c3ta12277h

Reference yield:

4-methyl-2-pentanone (108-10-1) + N-phenylphenylene-1,4-diamine (101-54-2) → C18H22N2 (63302-40-9)

Guidance literature:

In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 0.0833333h; Solvent;

Reference yield: 92.6%

C18H22N2 (63302-40-9) → N-(1,3-dimethylbutyl)-N'-phenyl-p-phenylenediamine (793-24-8)

Guidance literature:

With palladium on activated charcoal; hydrogen; In 5,5-dimethyl-1,3-cyclohexadiene; at 100 ℃; under 7500.75 Torr; Solvent; Temperature;

upstream raw materials:

4-methyl-2-pentanone

N-phenylphenylene-1,4-diamine

Downstream raw materials:

N-(1,3-dimethylbutyl)-N'-phenyl-p-phenylenediamine