2,4,10-Undecatrienoyl chloride, 7,9-dimethoxy-3,6,8-trimethyl-11-phenyl-, (2E,4E,6S,7S,8R,9S,10E)-

Base Information

Chemical Name:2,4,10-Undecatrienoyl chloride, 7,9-dimethoxy-3,6,8-trimethyl-11-phenyl-, (2E,4E,6S,7S,8R,9S,10E)-
CAS No.:633302-49-5
Molecular Formula:C22H29ClO3
Molecular Weight:376.923
Hs Code.:

Synonyms:

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Chemical Property of 2,4,10-Undecatrienoyl chloride, 7,9-dimethoxy-3,6,8-trimethyl-11-phenyl-, (2E,4E,6S,7S,8R,9S,10E)-

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Technology Process of 2,4,10-Undecatrienoyl chloride, 7,9-dimethoxy-3,6,8-trimethyl-11-phenyl-, (2E,4E,6S,7S,8R,9S,10E)-

There total 3 articles about 2,4,10-Undecatrienoyl chloride, 7,9-dimethoxy-3,6,8-trimethyl-11-phenyl-, (2E,4E,6S,7S,8R,9S,10E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tributyl((1E,3S,4S,5R,6S,7E)-4,6-dimethoxy-3,5-dimethyl-8-phenylocta-1,7-dienyl)stannane

: 633302-49-5
(2E,4E,10E)-(6S,7S,8R,9S)-7,9-Dimethoxy-3,6,8-trimethyl-11-phenyl-undeca-2,4,10-trienoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 80 percent / Ph₃As; NMP / Pd(dba)3

2.1: LiOH / tetrahydrofuran; H₂O

3.1: NaH

3.2: COCl₂

With 1-methyl-pyrrolidin-2-one; lithium hydroxide; triphenyl-arsane; sodium hydride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; water; 1.1: Stille coupling;
DOI:10.1021/ol017092x

Reference yield:

: 443123-81-7
(2E,4E,6S,7S,8R,9S,10E)-7,9-dimethoxy-3,6,8-trimethyl-11-phenylundeca-2,4,10-trienoic acid

: 633302-49-5
(2E,4E,10E)-(6S,7S,8R,9S)-7,9-Dimethoxy-3,6,8-trimethyl-11-phenyl-undeca-2,4,10-trienoyl chloride

Guidance literature:: (2E,4E,6S,7S,8R,9S,10E)-7,9-dimethoxy-3,6,8-trimethyl-11-phenylundeca-2,4,10-trienoic acid; With sodium hydride;

Further stages.;
DOI:10.1021/ol017092x

Reference yield:

: 405150-67-6
(2E,4E,6S,7S,8R,9S,10E)-methyl 7,9-dimethoxy-3,6,8-trimethyl-11-phenylundeca-2,4,10-trienoate

: 633302-49-5
(2E,4E,10E)-(6S,7S,8R,9S)-7,9-Dimethoxy-3,6,8-trimethyl-11-phenyl-undeca-2,4,10-trienoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiOH / tetrahydrofuran; H₂O

2.1: NaH

2.2: COCl₂

With lithium hydroxide; sodium hydride; In tetrahydrofuran; water;
DOI:10.1021/ol017092x