1H-Imidazole-1-carboxylic acid, 2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl] methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

Base Information

Chemical Name:1H-Imidazole-1-carboxylic acid, 2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl] methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester
CAS No.:633696-67-0
Molecular Formula:C28H36Cl2N4O5S
Molecular Weight:611.59
Hs Code.:

1H-Imidazole-1-carboxylic acid,
2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl]
methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

Synonyms:

Suppliers and Price of 1H-Imidazole-1-carboxylic acid, 2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl] methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1H-Imidazole-1-carboxylic acid, 2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl] methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Imidazole-1-carboxylic acid, 2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl] methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

There total 8 articles about 1H-Imidazole-1-carboxylic acid, 2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl] methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]butanoic acid

: 441295-92-7
4,5-dihydro-2-[4-[(methylamino)methyl]phenyl]-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

: 633696-67-0
2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl]methylamino]methyl]phenyl]-4,5-dihydro-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/jm2016057

Reference yield: 34.0%

: 633696-67-0
2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl]methylamino]methyl]phenyl]-4,5-dihydro-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:

Reference yield:

: 441295-89-2
[(4-cyanophenyl)methyl]methylcarbamic acid phenylmethyl ester

: 633696-67-0
2-[4-[[[4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxobutyl]methylamino]methyl]phenyl]-4,5-dihydro-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sulfur / 2 h / 100 °C

2: dmap / dichloromethane / 2 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr

4: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

With dmap; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; hydrogen; sulfur; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1021/jm2016057