1H-Imidazole-1-carboxylic acid, 2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo -2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

Base Information

Chemical Name:1H-Imidazole-1-carboxylic acid, 2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo -2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester
CAS No.:633696-69-2
Molecular Formula:C28H34Cl2N4O5S
Molecular Weight:609.574
Hs Code.:

1H-Imidazole-1-carboxylic acid,
2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo
-2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl
ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Imidazole-1-carboxylic acid, 2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo -2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

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Technology Process of 1H-Imidazole-1-carboxylic acid, 2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo -2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester

There total 9 articles about 1H-Imidazole-1-carboxylic acid, 2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo -2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-(2E)-2-butenoic acid

: 441295-92-7
4,5-dihydro-2-[4-[(methylamino)methyl]phenyl]-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

: 633696-69-2
2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo-2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/jm2016057

Reference yield: 74.0%

: 633696-69-2
2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo-2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:

Reference yield:

: 441295-89-2
[(4-cyanophenyl)methyl]methylcarbamic acid phenylmethyl ester

: 633696-69-2
2-[4-[[[(2E)-4-[[(2,4-dichloro-3-methylphenyl)sulfonyl]methylamino]-1-oxo-2-butenyl]methylamino]methyl]phenyl]-4,5-dihydro-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sulfur / 2 h / 100 °C

2: dmap / dichloromethane / 2 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr

4: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

With dmap; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; hydrogen; sulfur; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1021/jm2016057