2-hydroxy-N-(1-phenylcyclohexyl)piperidine

Base Information

• Chemical Name: 2-hydroxy-N-(1-phenylcyclohexyl)piperidine
• CAS No.: 83400-97-9
• Molecular Formula: C17H25 N O
• Molecular Weight: 259.392
• Hs Code.: 2933399090
• Mol file: 83400-97-9.mol

Synonyms:N-[1-(2-Hydroxyphenyl)cyclohexyl]piperidine

Chemical Property of 2-hydroxy-N-(1-phenylcyclohexyl)piperidine

Chemical Property:

• Vapor Pressure: 3.95E-06mmHg at 25°C
• Boiling Point: 374.2°C at 760 mmHg
• Flash Point: 167.9°C
• PSA: 23.47000
• Density: 1.086g/cm³
• LogP: 3.97540

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-hydroxy-N-(1-phenylcyclohexyl)piperidine

There total 2 articles about 2-hydroxy-N-(1-phenylcyclohexyl)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phencyclidine (77-10-1) → 4-Phenyl-4-piperidinocyclohexanol (60756-83-4) + 2-(1-Piperidin-1-yl-cyclohexyl)-phenol (83400-97-9) + 3-hydroxy-1-(1-phenylcyclohexyl)piperidine (94852-59-2) + 1-(1-phenlcyclohexyl)-3-piperidine (123041-84-9)

Guidance literature:

With meso-tetraphenylporphyrin iron(III) chloride; iodosylxylene; In benzene; for 1h; Yield given. Further byproducts given; var. reag.: cumene hydroperoxide;

DOI:10.1248/cpb.37.1788

Reference yield:

Phencyclidine (77-10-1) → 4-(1-Piperidin-1-yl-cyclohexyl)-phenol (66568-88-5) + 4-Phenyl-4-piperidinocyclohexanol (60756-83-4) + N-[1-(3-hydroxyphenyl)cyclohexyl]piperidine (79787-43-2) + 2-(1-Piperidin-1-yl-cyclohexyl)-phenol (83400-97-9) + 5-pentanoic acid (77160-83-9) + 3-hydroxy-1-(1-phenylcyclohexyl)piperidine (94852-59-2)

Guidance literature:

With perchloric acid; ferrous perchlorate; dihydrogen peroxide; In water; acetonitrile; at 37 ℃; for 1h; Product distribution; var. reag.: O₂ and ascorbic acid; Fe(III)TPPCl and iodosylxylene or cumene hydroperoxide;Fe(III)TPPCl,O₂ and Zn, AcOH; liver microsomes and NADPH, O₂;

DOI:10.1248/cpb.37.1788

upstream raw materials:

Phencyclidine

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