Carbamic acid, [(1R)-2-(2-benzothiazolylsulfonyl)-1-[(4S,5R)-2,2-dimethyl-5-tetradecyl- 1,3-dioxolan-4-yl]ethyl]-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, [(1R)-2-(2-benzothiazolylsulfonyl)-1-[(4S,5R)-2,2-dimethyl-5-tetradecyl- 1,3-dioxolan-4-yl]ethyl]-, phenylmethyl ester
CAS No.:634587-47-6
Molecular Formula:C36H52N2O6S2
Molecular Weight:672.951
Hs Code.:

Synonyms:

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Chemical Property of Carbamic acid, [(1R)-2-(2-benzothiazolylsulfonyl)-1-[(4S,5R)-2,2-dimethyl-5-tetradecyl- 1,3-dioxolan-4-yl]ethyl]-, phenylmethyl ester

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Technology Process of Carbamic acid, [(1R)-2-(2-benzothiazolylsulfonyl)-1-[(4S,5R)-2,2-dimethyl-5-tetradecyl- 1,3-dioxolan-4-yl]ethyl]-, phenylmethyl ester

There total 6 articles about Carbamic acid, [(1R)-2-(2-benzothiazolylsulfonyl)-1-[(4S,5R)-2,2-dimethyl-5-tetradecyl- 1,3-dioxolan-4-yl]ethyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 634587-46-5
C₃₆H₅₂N₂O₄S₂

: 634587-47-6
C₃₆H₅₂N₂O₆S₂

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 554-62-1
D-ribo-phytosphingosine

: 634587-47-6
C₃₆H₅₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydrogencarbonate / 1,4-dioxane; ethyl acetate / 20 °C

2: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 1 h / 0 °C

3: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 4 h / 20 °C

5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3 h / 20 °C

6: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

With dmap; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 634587-40-9
(2S,3R,4R)-1-O-tert-butyldimethysilyl-2-benzyloxycarbonylamino-1,3,4-octadecanetriol

: 634587-47-6
C₃₆H₅₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 4 h / 20 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3 h / 20 °C

4: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane;