Hexanedinitrile, 2-(3,5-dimethylphenyl)-

Base Information

Chemical Name:Hexanedinitrile, 2-(3,5-dimethylphenyl)-
CAS No.:634603-12-6
Molecular Formula:C14H16N2
Molecular Weight:212.294
Hs Code.:

Synonyms:

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Chemical Property of Hexanedinitrile, 2-(3,5-dimethylphenyl)-

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Technology Process of Hexanedinitrile, 2-(3,5-dimethylphenyl)-

There total 1 articles about Hexanedinitrile, 2-(3,5-dimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 628-20-6
4-Chlorobutyronitrile

: 39101-54-7
3,5-dimethylphenylacetonitrile

: 634603-12-6
2-(3,5-dimethylphenyl)hexanedinitrile

Guidance literature:: 4-Chlorobutyronitrile; 3,5-dimethylphenylacetonitrile; With sodium ethanolate; Diethyl carbonate; Heating;

With potassium hydroxide; In ethanol; for 0.5h; Further stages.; Heating;
DOI:10.1039/b303658h

Reference yield: 93.0%

: 634603-12-6
2-(3,5-dimethylphenyl)hexanedinitrile

: 634603-14-8
2-amino-1-cyano-3-(3,5-dimethylphenyl)cyclopent-1-ene

Guidance literature:: With sodium hydride; In 1,4-dioxane; for 2.5h; Heating;
DOI:10.1039/b303658h

Reference yield:

: 634603-12-6
2-(3,5-dimethylphenyl)hexanedinitrile

: 7-(3,5-dimethylphenyl)-1-ethoxymethyl-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / NaH / dioxane / 2.5 h / Heating

2: 55 percent / glacial acetic acid; aq. HCl / 6 h / Heating

3: 35 percent / 3 h / 55 - 130 °C

4: 90 percent / aq. NH₃ / 24 h / Heating

5: 80 percent / N,O-bis(trimethylsilyl)acetamide / CHCl₃ / 5 h / 20 °C

With hydrogenchloride; ammonium hydroxide; N,O-bis-(trimethylsilyl)-acetamide; sodium hydride; acetic acid; In 1,4-dioxane; chloroform; 1: Thorpe-Ziegler reaction;
DOI:10.1039/b303658h