1-(4-Methylphenyl)-3-phenyl-3-sulfanylidenepropan-1-one

Base Information

Chemical Name:1-(4-Methylphenyl)-3-phenyl-3-sulfanylidenepropan-1-one
CAS No.:63523-21-7
Molecular Formula:C₁₆H₁₄OS
Molecular Weight:254.353
Hs Code.:
DSSTox Substance ID:DTXSID30490556
Wikidata:Q82334381

Synonyms:63523-21-7;1-(4-Methylphenyl)-3-phenyl-3-sulfanylidenepropan-1-one;DTXSID30490556

Suppliers and Price of 1-(4-Methylphenyl)-3-phenyl-3-sulfanylidenepropan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(4-Methylphenyl)-3-phenyl-3-sulfanylidenepropan-1-one

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:254.07653624
Heavy Atom Count:18
Complexity:296

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)CC(=S)C2=CC=CC=C2

Technology Process of 1-(4-Methylphenyl)-3-phenyl-3-sulfanylidenepropan-1-one

There total 1 articles about 1-(4-Methylphenyl)-3-phenyl-3-sulfanylidenepropan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 936-61-8
Thiobenzoic acid O-ethyl ester

: 122-00-9
para-methylacetophenone

: 63523-21-7
PhCSCH₂COC₆H₄CH₃-p

Guidance literature:: Multistep reaction; (i) NaNH₂, Et₂O, (ii) /BRN= 1072494/;
DOI:10.1055/s-1977-24342

Reference yield: 86.0%

: indium isopropoxide

: 63523-21-7
PhCSCH₂COC₆H₄CH₃-p

: In(C₆H₅CSCHCOC₆H₄CH₃)3

Guidance literature:: In benzene; byproducts: isopropanol; benzene soln. of the ligand mixed a benzene soln. of the propoxide (1 : 3 molar ratio), colour change from red to yellow, refluxed (fractionating column), estimating the alcohol in the azeotrope; evapn., drying in vac., recrystn. (benzene/hexane), elem. anal.;