2,3-Bis(4-methylphenyl)-2,3-dihydrophthalazine-1,4-dione

Base Information

Chemical Name:2,3-Bis(4-methylphenyl)-2,3-dihydrophthalazine-1,4-dione
CAS No.:63546-89-4
Molecular Formula:C₂₂H₁₈N₂O₂
Molecular Weight:342.397
Hs Code.:2933990090
DSSTox Substance ID:DTXSID40702930
Nikkaji Number:J131.440H
Wikidata:Q82634960

Synonyms:63546-89-4;1,4-Phthalazinedione, 2,3-dihydro-2,3-bis(4-methylphenyl)-;DTXSID40702930;2,3-Bis(4-methylphenyl)-2,3-dihydrophthalazine-1,4-dione;2,3-Dihydro-2,3-bis(4-methylphenyl)-1,4-phthalazinedione

Suppliers and Price of 2,3-Bis(4-methylphenyl)-2,3-dihydrophthalazine-1,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,3-Bis(4-methylphenyl)-2,3-dihydrophthalazine-1,4-dione

Chemical Property:

PSA：44.00000
LogP:3.75840
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:342.136827821
Heavy Atom Count:26
Complexity:484

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N2C(=O)C3=CC=CC=C3C(=O)N2C4=CC=C(C=C4)C

Technology Process of 2,3-Bis(4-methylphenyl)-2,3-dihydrophthalazine-1,4-dione

There total 4 articles about 2,3-Bis(4-methylphenyl)-2,3-dihydrophthalazine-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 20172-08-1
N¹,N²-di-p-tolylphthalamide

: 63546-89-4
2,3-di(4-methylphenyl)-2,3-dihydrophthalazin-1,4-dione

Guidance literature:: With tert-butylammonium hexafluorophosphate(V); Electrolysis;
DOI:10.1002/chem.201705578

Reference yield:

: 88-95-9
Phthaloyl dichloride

: 637-47-8
1,2-di(p-tolyl)hydrazine

: 63546-89-4
2,3-di(4-methylphenyl)-2,3-dihydrophthalazin-1,4-dione

Guidance literature:: With 2,3-Dimethylaniline; at 20 ℃;

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 88-95-9
Phthaloyl dichloride

: 63546-89-4
2,3-di(4-methylphenyl)-2,3-dihydrophthalazin-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 16 h / 20 °C

2: tert-butylammonium hexafluorophosphate(V) / Electrolysis

With tert-butylammonium hexafluorophosphate(V); In diethyl ether;
DOI:10.1002/chem.201705578