1-(2,4-Dinitrophenyl)-2-heptylidenehydrazine

Base Information

Chemical Name:1-(2,4-Dinitrophenyl)-2-heptylidenehydrazine
CAS No.:2074-05-7
Molecular Formula:C13H18 N4 O4
Molecular Weight:294.31
Hs Code.:2928000090
NSC Number:6128
Mol file:2074-05-7.mol

Synonyms:1-(2,4-dinitrophenyl)-2-heptylidenehydrazine;2074-05-7;Heptanal 2,4-dinitrophenylhydrazone;N-[(E)-heptylideneamino]-2,4-dinitroaniline;HEPTALDEHYDE (DNPH DERIVATIVE);Heptanal, (2,4-dinitrophenyl)hydrazone;NSC6128;Heptaldehyde, 2,4-dinitrophenyl hydrazone;Heptanal-2,4-dinitrophenylhydrazone 100 microg/mL in Acetonitrile;HAPHKPXFYXPWDK-NTEUORMPSA-N;NSC-6128;AKOS024319319;(1E)-Heptanal (2,4-dinitrophenyl)hydrazone;J-013577;Heptaldehyde-DNPH, vial of 10 mg, analytical standard;Heptanal 2,4-dinitrophenylhydrazone, analytical standard

Suppliers and Price of 1-(2,4-Dinitrophenyl)-2-heptylidenehydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 1-(2,4-Dinitrophenyl)-2-heptylidenehydrazine

Chemical Property:

Vapor Pressure:8.97E-08mmHg at 25°C
Melting Point:99-102 °C
Boiling Point:435.1°Cat760mmHg
Flash Point:217°C
PSA：116.03000
Density:1.26g/cm³
LogP:4.99050
Storage Temp.:?20°C
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:7
Exact Mass:294.13280507
Heavy Atom Count:21
Complexity:364

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CCCCCCC=NNC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-]
Isomeric SMILES:CCCCCC/C=N/NC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1-(2,4-Dinitrophenyl)-2-heptylidenehydrazine

There total 6 articles about 1-(2,4-Dinitrophenyl)-2-heptylidenehydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1117-86-8
1,2-octandiol

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 2074-05-7
heptanal 2,4-dinitrophenylhydrazone

Guidance literature:: 1,2-octandiol; With cerium(III) chloride heptahydrate; tetrabutyl-ammonium chloride; In [D₃]acetonitrile; at 20 ℃; for 18h; Molecular sieve; Sealed tube; Irradiation;

(2,4-dinitro-phenyl)-hydrazine; With sulfuric acid; In ethanol; water; at 0 - 20 ℃;
DOI:10.1039/c8cc09208g

Reference yield:

: 122-32-7
trioleoylglycerol

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 53448-07-0,71277-05-9,2463-77-6
2-undecenal

: 2074-05-7
heptanal 2,4-dinitrophenylhydrazone

: 4237-03-0
Δ²-Decenal-(2,4-dinitro-phenylhydrazon)

: 1527-95-3
decanal (2,4-dinitrophenyl)hydrazone

: 1527-97-5
1-(hexylidene)-2-(2,4-dinitrophenyl)hydrazine

: 1726-77-8
octanal (2,4-dinitrophenyl)hydrazone

: 2348-19-8,74335-75-4,74335-76-5
nonanal (2,4-dinitrophenyl)hydrazone

Guidance literature:: trioleoylglycerol; With air; at 120 ℃; for 10h;

(2,4-dinitro-phenyl)-hydrazine; In acetonitrile; for 1h; Darkness;
DOI:10.1007/s00706-017-2036-3

Reference yield:

: 78483-77-9
1,3-dimethyl-2-hexylbenzimidazolium iodide

: 2074-05-7
heptanal 2,4-dinitrophenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol; sodium / 0.75 h / 20 °C / Inert atmosphere

1.2: 1 h / 60 °C / pH 4 - 5 / Inert atmosphere

2.1: ethanol; water

With ethanol; sodium; In ethanol; water;
DOI:10.1002/cjoc.201190110